GC Analysis of Derivatized Chlorinated Acetic Acids

Thermo Scientific Reagents, Solvents and Accessories • Gas Chromatography • High Performance Liquid Chromatography • Mass Spectrometry Table of Contents Thermo Scientific Products for GC and HPLC Amino Acid Analysis 33-43 Derivatization Reagents for Specific Functional Groups 1-2 Derivatization Reagents…

Anila I Khan, Thermo Fisher Scientific, Runcorn, Cheshire, UK Key Words Derivatization reagent, silylation, N-methyl-N–(trimethylsilyl) trifluoroacetamide (MSTFA), L-alanine, L-leucine, L-lysine, amino acid Abstract The derivatization of amino acids was achieved using the MSTFA silylation reagent. The TFA derivatized compounds were…

Bulletin 909A Guide to Derivatization Reagents for GC A large number of reagents are used to prepare derivatives for gas chromatography, but most of the derivatization reactions fit into one of three categories: acylation, alkylation, or silylation. This bulletin describes…

Anila I Khan, Thermo Fisher Scientific, Runcorn, Cheshire, UK Key Words Derivatization reagent, silylation, N-methyl-N–(trimethylsilyl) trifluoroacetamide (MSTFA), L-alanine, L-leucine, L-lysine, amino acid Abstract The derivatization of amino acids was achieved using the MSTFA silylation reagent. The TFA derivatized compounds were…