<p><strong>Taťána Gazárková is currently a&nbsp;postdoctoral fellow in the Laboratory of Antibiotic Resistance and Microbial Metabolomics. During her doctoral studies, she focused on chromatography and mass spectrometry. Recently, she was awarded second place in the “Sanofi Prize for Pharmacy 2026” competition.</strong></p><p><strong>Taťána Gazárková </strong>is currently a&nbsp;postdoctoral fellow in the <strong>Laboratory of Antibiotic Resistance and Microbial Metabolomics</strong>. During her doctoral studies, she focused on chromatography and mass spectrometry. Recently, she was awarded second place in the <strong>“Sanofi Prize for Pharmacy 2026” </strong>competition, which is awarded by the<strong> French Embassy in the Czech Republic</strong> for her dissertation – Steroid Analysis Using Modern Chromatographic and Mass Spectrometry Techniques: From Fundamental Studies to Targeted Bioanalytical Applications (supervisor: <strong>Lucie Nováková, Charles University</strong>).&nbsp;</p><h5><strong>What makes this field particularly exciting or unique in your view?</strong></h5><p>What I&nbsp;enjoy about analytical chemistry is that, to a&nbsp;certain extent, it is a&nbsp;kind of detective work. You are often looking for ways to “make the invisible visible”. In other words, extract the information you are interested in from a&nbsp;complex sample and then interpret it correctly. What also appeals to me about bioanalytical chemistry is its interdisciplinary nature. It brings together analytical chemistry, biochemistry, biology and medicine, which means that you need to be able not only to translate a&nbsp;biological or clinical question into a&nbsp;measurable analytical experiment, but also to place the resulting data back into a&nbsp;broader biological context. This combination of different perspectives is probably what I&nbsp;enjoy most about the field. At the same time, there is still plenty of room for fundamental research, ranging from studying analytical techniques themselves and improving them to developing new methodological approaches.</p><h5><strong>How did you end up at the </strong><a target="_blank" rel="noopener noreferrer" href="https://mbu.cas.cz/en/research/laboratory-of-antibiotic-resistance-and-microbial-metabolomics"><strong>Laboratory of Antibiotic Resistance and Microbial Metabolomics</strong></a><strong>, and what project are you currently working on?</strong></h5><p>I came to the Institute of Microbiology through a&nbsp;joint project between<strong> Dr Zdeněk Kameník and Assoc. Prof. Jan Bobek from the First Faculty of Medicine, Charles University</strong>. For me, it was also an opportunity to move from targeted analysis and the study of chromatographic techniques towards untargeted metabolomics and new biological questions.</p><p>In the project, we are trying to identify new biologically active compounds that would be effective, particularly against pathogenic fungi. As a&nbsp;potential source of such compounds, we study streptomycetes, bacteria known for their ability to produce a&nbsp;wide range of biologically active compounds, including many antibiotics that are currently in clinical use. We focus on less-explored host-associated streptomycetes, in which we had already observed antifungal activity in previous experiments. We are especially interested in strains active against Candida albicans whose activity cannot be explained by the presence of a&nbsp;known bioactive compound. These strains may represent an interesting source of novel compounds. We then integrate the results of untargeted metabolomic analyses with genomic analyses, which allows us to obtain a&nbsp;more comprehensive view of the biosynthetic potential of selected strains.</p><h5><strong>You also took part in this year’s Vědafest, a&nbsp;science outreach event for the public. What was it like?</strong></h5><p>I already had some experience with science outreach through events such as Researchers’ Night and the Science Fair at my previous institution, but this year’s Vědafest was still new to me in some ways. This time, I&nbsp;was presenting a&nbsp;field that I&nbsp;myself had entered only relatively recently. It was therefore more challenging to find the right analogies and explain the essence of the topic in a&nbsp;way that was simple, yet precise and scientifically accurate. At the same time, that was exactly what made it inspiring. It forces you to look at your own work from a&nbsp;different perspective. What I&nbsp;enjoyed most was the spontaneity and curiosity of the children, who often came up with questions that would never even occur to an adult.</p><h5><strong>What are the biggest challenges you face on your scientific journey, and what helps you overcome them?</strong></h5><p>One of the greatest, but at the same time most interesting, challenges is, in my view, the uncertainty that is inseparably linked to research. For a&nbsp;long time, you often do not know whether you have taken the right direction in addressing a&nbsp;particular question or whether you will ultimately manage to find that figurative final piece of the puzzle. At the same time, this uncertainty is precisely what makes science exciting for me.</p><p>Another major challenge, particularly in interdisciplinary projects, is communication. It is important from the very formulation of a&nbsp;hypothesis and the planning of experiments through to the interpretation of results, including negative ones, and placing them in a&nbsp;broader context. To some extent, every field has its own language, and finding a&nbsp;common understanding is not always straightforward. Personally, I&nbsp;find it very helpful to be able to discuss problems with colleagues on an ongoing basis, whether individually or during regular laboratory seminars. One of the major strengths of our current group is its interdisciplinary nature, which allows me to look at the same problem from several different perspectives. It is also important for me not to lose my curiosity, because that is ultimately what leads us to ask further questions.</p><h5><strong>What are your plans after completing your PhD?</strong></h5><p>After finishing my PhD, I&nbsp;decided that I&nbsp;do not need to have everything that comes next precisely mapped out straight away. I&nbsp;would like to keep different options open for a&nbsp;while and continue building on my experience in analytical chemistry, while at the same time connecting it with other areas that have a&nbsp;biological or medical relevance. I&nbsp;believe that we can keep learning throughout our lives, so I&nbsp;am quite curious to see where the next stage of my journey will take me.</p><p><i>Thank you for the interview!</i></p>

Interview: What Drew Postdoc Taťána Gazárková to Analytical Chemistry

<p><strong>Per- and polyfluoroalkyl substances (PFAS) have earned the moniker "forever chemicals" due to their extreme persistence in the environment. Their detection is crucial for protecting public health and the environment as these synthetic compounds continue to pose significant challenges worldwide. This comprehensive exploration examines why PFAS detection matters, current detection methods, and future directions in addressing PFAS contamination.</strong></p><h3><strong>Understanding PFAS and Their Health Impacts</strong></h3><p>PFAS are a class of synthetic organic compounds with diverse structures, properties, and uses. Despite their diversity, all PFAS contain perfluoroalkyl moieties that are extremely resistant to environmental and metabolic degradation [1]. This high persistence is a defining characteristic that makes PFAS management particularly challenging.</p><h3><strong>Documented Health Effects</strong></h3><p>Current scientific research has linked PFAS exposure to numerous adverse health outcomes:</p><ul><li>Reproductive effects including decreased fertility and increased high blood pressure in pregnant women [8]</li><li>Developmental effects in children such as low birth weight, accelerated puberty, and behavioral changes [8]</li><li>Reduced immune system function, including decreased vaccine response</li><li>Interference with natural hormones and endocrine disruption</li><li>Increased cholesterol levels and obesity risk</li><li>Increased risk of several cancers, including prostate, kidney, testicular, oral cavity/pharynx, brain, and endocrine cancers [3]</li></ul><p>A 2023 study linked PFAS-contaminated water with up to a <strong>33% increase in cancer incidence</strong> in affected areas [3]. The study compared regions with elevated PFAS levels to cancer data from the National Cancer Institute, finding higher incidences of various cancers after controlling for factors like smoking and obesity.</p><h3><strong>Environmental Persistence and Contamination</strong></h3><p>The extreme persistence of PFAS represents a fundamental concern for environmental management. PFAS are considered the most environmentally persistent substances among organic chemicals [7]. This persistence means that even if all PFAS uses were immediately phased out, existing contamination would continue to affect ecosystems and water supplies for generations.</p><p>A 2023 study at a military fire training site estimated that PFAS contamination will persist for centuries without remediation [7]. The research found that terminal PFAS still exceed regulatory limits by 2000-fold decades after aqueous film-forming foam (AFFF) use ceased, with precursors accounting for around half of the extractable organofluorine across years.</p><h3><strong>Current Detection Methods</strong></h3><h4><strong>EPA Standardized Methods</strong></h4><p>The<strong> Environmental Protection Agency (EPA</strong>) has developed several standardized methods for PFAS detection, each with specific applications and capabilities:</p><h5><strong>EPA Method 533</strong></h5><p><a target="_blank" rel="noopener noreferrer" href="https://blog.organomation.com/blog/epa-533-drying-down-pfas-samples-after-spe"><strong>EPA Method 533</strong></a> focuses on "short chain" PFAS with carbon chain lengths of<strong> C4 to C12</strong>. Released in December 2019, this method complements Method 537.1 and includes several key features:</p><ul><li>Uses isotope dilution quantification approach with extracted internal standards, which reduces overall analytical uncertainty</li><li>Employs weak anion exchange solid phase extraction cartridges as opposed to polystyrene divinylbenzene used in 537.1</li><li>Can analyze 25 PFAS compounds, including additional short-chain PFAS that were not apart of Method 537.1</li><li>Allows for longer holding times: 28 days to extraction and 28 days to analyze (compared to 14 days to extraction in Method 537.1)</li><li>Uses ammonium acetate as a preservative (versus Trisma in Method 537.1) [1]</li></ul><h5><strong>EPA Method 537/537.1</strong></h5><p><a target="_blank" rel="noopener noreferrer" href="https://blog.organomation.com/blog/sample-concentration-epa-method-537-pfas-determination"><strong>EPA Method 537 </strong></a>was first published in 2009 for the determination of 14 PFAS in drinking water [6]. It was later updated to Method 537.1 in 2018 (with editorial updates in 2020) to expand its capabilities:</p><ul><li>Uses<a target="_blank" rel="noopener noreferrer" href="https://www.organomation.com/what-is-solid-phase-extraction-spe"><strong> solid phase extraction (SPE) </strong></a>and<a target="_blank" rel="noopener noreferrer" href="https://www.organomation.com/preparing-samples-for-lc-ms/ms-analysis"><strong> liquid chromatography/tandem mass spectrometry (LC-MS/MS)</strong></a></li><li>Method 537.1 expanded detection to 18 PFAS compounds, including HFPO-DA (one component of GenX technology)</li><li>Utilizes styrene-divinylbenzene (SDVB) media for extraction</li><li>Requires samples to be extracted within 14 days and analyzed within 28 days</li><li>Methanol is used to elute the extracts. This should then be reconstituted with a 96:4 methanol:water mixture [1]</li></ul><p>Together, Methods 533 and 537.1 can detect a total of <strong>29 unique PFAS compounds in drinking water </strong>and are approved for monitoring under the fifth Unregulated Contaminant Monitoring Rule (UCMR 5) and the PFAS National Primary Drinking Water Regulation [1] [3].</p><h5><strong>EPA Method 1633</strong></h5><p><a target="_blank" rel="noopener noreferrer" href="https://blog.organomation.com/blog/preparing-diverse-sample-matrices-for-epa-method-1633"><strong>EPA Method 1633</strong></a>, released in 2024, represents a significant advancement in PFAS analysis:</p><ul><li>Developed for the analysis of <strong>40 PFAS compounds </strong>in various matrices, including surface water, groundwater, wastewater, soil, biosolids, sediment, landfill leachate, and fish tissue</li><li>Expands beyond the drinking water focus of Methods 533 and 537.1</li><li>Provides a standardized approach that may replace modified drinking water methods (i.e., modified EPA 537) that were previously used for non-drinking water matrices [1]</li></ul><h4><strong>Conventional Analytical Techniques</strong></h4><p>The gold standard for PFAS analysis involves chromatographic techniques coupled with mass spectrometry:</p><ul><li>Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS) is the most widely used method for PFAS analysis, offering high sensitivity and specificity [1]</li><li>High-Resolution Mass Spectrometry (HRMS) allows for rapid detection and identification of PFAS species at very low concentrations [5]</li></ul><p>These techniques can detect PFAS at parts per trillion (ppt) levels, which is essential given the low concentrations at which PFAS can cause health effects [1]. However, these methods require sophisticated equipment, specialized training, and significant financial resources, making them inaccessible in many regions, particularly in developing countries.</p><h4><strong>Emerging Detection Technologies</strong></h4><p>Several innovative approaches are being developed to address the limitations of conventional methods:</p><ul><li>Electrochemical biosensors using modified electrodes have shown promise for selective PFAS detection with low detection limits [2]</li><li>Surface-Enhanced Raman Spectroscopy (SERS) uses metallic nanoparticles and can be made into a portable method for on-site testing [1]</li><li>Molecular imprinted polymers (MIPs) offer thermal and physical stability, reusability, and low-cost synthesis for PFAS detection [6]</li></ul><p>These emerging technologies aim to provide more accessible, field-deployable, and cost-effective alternatives to traditional laboratory-based methods.</p><h3><strong>Challenges in PFAS Detection</strong></h3><h4><strong>Analytical Challenges</strong></h4><p>Detecting PFAS presents several technical challenges:</p><ul><li>The ubiquity of PFAS in laboratory equipment and accessories can lead to background contamination when measuring at parts-per-trillion levels [1]</li><li>Many components in liquid chromatographs, mass spectrometers, and solid-phase extraction systems contain materials that can leach PFAS compounds [9]</li><li>The vast number of PFAS (thousands of compounds) makes comprehensive detection difficult, as analytical standards are only available for a small subset [1]</li><li>Complex matrices like food and environmental samples require sophisticated sample preparation techniques</li></ul><h4><strong>Global Disparities in Detection Capabilities</strong></h4><p>Access to PFAS detection technology varies significantly worldwide:</p><ul><li>Many developing regions, particularly in Africa, lack adequately equipped laboratories with the necessary instrumentation to detect and measure PFAS</li><li>There is often a scarcity of qualified professionals with experience in PFAS analysis in these regions</li><li>The high cost of acquiring and maintaining sophisticated analytical instruments presents a substantial obstacle to conducting extensive PFAS investigations in resource-limited settings [1]</li><li>Competing priorities such as infectious diseases, poverty, and food security often divert attention and resources from environmental pollutants like PFAS</li></ul><h4><strong>Regulatory Landscape and Compliance</strong></h4><p>The regulatory framework for PFAS is evolving rapidly worldwide:</p><ul><li>The EPA finalized Section 8(a)(7) of the Toxic Substances Control Act in September 2024, requiring manufacturers and importers to report on their use of PFAS since 2011 [10]</li><li>Electronic reporting for PFAS will open on July 11, 2025, with final reporting deadlines in 2026</li><li>Companies must report detailed information including chemical identity, production volumes, industrial and consumer products, worker exposure, and disposal methods [10]</li></ul><p>These regulations are driving demand for more effective and accessible PFAS detection methods to ensure compliance and protect public health.</p><h3><strong>Future Directions in PFAS Detection</strong></h3><h4><strong>Technological Advancements</strong></h4><p>The future of PFAS detection lies in developing more accessible, sensitive, and comprehensive methods:</p><ul><li>Non-targeted screening methods that can identify unknown PFAS compounds without requiring analytical standards for each specific compound</li><li>Total fluorine analysis techniques like Adsorbable Organic Fluorine and Total Oxidizable Precursor Assay that can quantify the presence of fluorine atoms within a sample [1]</li><li>Portable sensors and field-deployable technologies that enable on-site monitoring and rapid response to contamination events</li><li>AI-driven solutions that can improve data analysis and interpretation for complex PFAS mixtures</li></ul><h4><strong>Collaborative Approaches</strong></h4><p>Addressing the global challenge of PFAS detection requires coordinated efforts:</p><ul><li>International partnerships between researchers in developed and developing regions to enhance expertise and capacity building</li><li>Standardization of analytical methods to ensure consistency and comparability of results across different laboratories and regions</li><li>Open data sharing and collaboration across countries to leverage collective knowledge and resources</li><li>Integration of PFAS monitoring into broader environmental and public health surveillance systems</li></ul><h3><strong>Conclusion</strong></h3><p>The detection of PFAS is not merely a technical challenge but a critical public health and environmental imperative [1]. As these "forever chemicals" continue to persist in our environment, developing effective, accessible, and comprehensive detection methods becomes increasingly important. By advancing detection technologies, strengthening regulatory frameworks, and fostering global collaboration, we can better understand, monitor, and ultimately mitigate the impacts of PFAS contamination.</p><p>The EPA's standardized methods (533, 537.1, and 1633) provide crucial tools for monitoring PFAS in various environmental matrices, but continued innovation is needed to address the full spectrum of PFAS compounds and to make detection more accessible globally [1] [6]. The path forward requires sustained investment in research and development, capacity building in resource-limited settings, and a commitment to environmental justice that ensures all communities have access to the tools and information needed to protect themselves from PFAS exposure. Only through such comprehensive approaches can we hope to address the complex challenges posed by these persistent pollutants.</p><p><span>Be sure to check out our other installments of our&nbsp;</span><a target="_blank" rel="noopener noreferrer" href="https://blog.organomation.com/blog/introducing-our-environmental-contaminants-series-making-sense-of-the-alphabet-soup"><span>Environmental Contaminant Series</span></a><span>&nbsp;covering&nbsp;</span><a target="_blank" rel="noopener noreferrer" href="https://blog.organomation.com/blog/the-importance-of-detecting-persistent-organic-pollutants-pops"><span>Persistent Organic Pollutants (POPs)</span></a><span>,&nbsp;</span><a target="_blank" rel="noopener noreferrer" href="https://blog.organomation.com/blog/the-importance-of-detecting-polycyclic-aromatic-hydrocarbons-pahs"><span>Polycyclic Aromatic Hydrocarbons (PAHs)</span></a><span>,&nbsp;</span><a target="_blank" rel="noopener noreferrer" href="https://blog.organomation.com/blog/the-importance-of-detecting-semi-volatile-organic-compounds-svocs"><span>Semi-Volatile Organic Compounds (SVOCs)</span></a><span>, and </span><a target="_blank" rel="noopener noreferrer" href="https://blog.organomation.com/blog/the-importance-of-detecting-polychlorinated-biphenyls-pcbs"><span>Polychlorinated Biphenyls (PCBs)</span></a><span>.</span></p>

The Importance of Detecting Per- and Polyfluoroalkyl Substances (PFAS)

<p><strong>Our Library never stops expanding. What are the most recent contributions to LabRulezICPMS Library in the week of 31st August 2026? Check out new documents from the field of spectroscopy/spectrometry and related techniques!</strong></p><blockquote><p><span style="font-size:20px;">👉 </span><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library"><span style="font-size:20px;"><strong>SEARCH THE LARGEST REPOSITORY OF DOCUMENTS ABOUT SPECTROSCOPY/SPECTROMETRY RELATED TECHNIQUES</strong></span></a></p></blockquote><blockquote><p><strong>👉 Need info about different analytical techniques?</strong> Peek into <a target="_blank" rel="noopener noreferrer" href="https://lcms.labrulez.com/library"><strong>LabRulezLCMS</strong></a> or <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/library"><strong>LabRulezGCMS</strong></a> libraries.</p></blockquote><p>This week we bring you brochures by <strong>Agilent Technologies </strong>and<strong> Waters Corporation </strong>and application notes by <strong>Shimadzu </strong>and<strong> Thermo Fisher Scientific!</strong></p><h3><strong>1. Agilent Technologies: Agilent OpenLab ICP-MS Software</strong></h3><p><strong>Simplify every step of ICP-MS analysis</strong></p><p><strong>For Agilent </strong><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/icpms/library?mainauthorItems=10&amp;search=7800"><strong>7800</strong></a><strong>, </strong><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/icpms/library?mainauthorItems=10&amp;search=7850"><strong>7850</strong></a><strong>, and </strong><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/icpms/library?mainauthorItems=10&amp;search=7900"><strong>7900</strong></a><strong> ICP-MS systems, and Agilent </strong><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/icpms/library?mainauthorItems=10&amp;search=8900"><strong>8900</strong></a><strong> and </strong><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/icpms/library?mainauthorItems=10&amp;search=9500"><strong>9500 ICP-QQQ</strong></a><strong> systems.</strong></p><ul><li>Brochure</li><li><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/pdf/br_openlab_icp_ms_software_5994_9288en_agilent_05f01dcdef.pdf"><strong>Full PDF for download</strong></a><strong>&nbsp;</strong></li></ul><p>The brochure introduces <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/icpms/library?mainauthorItems=10&amp;search=OpenLab+ICP-MS+Software"><strong>Agilent OpenLab ICP-MS Software</strong></a>, designed to simplify routine operation and data handling for <strong>Agilent 7800, 7850, and 7900 ICP-MS systems</strong> and the <strong>8900</strong> and <strong>9500</strong> <strong>ICP-QQQ systems</strong>. The software supports the complete analytical workflow—from checking instrument readiness and creating batches to acquisition, data review, reporting, and compliance. A central dashboard provides an overview of system status, maintenance requirements, instrument health, and utilization, while Smart EMF and post-run performance checks help users identify when maintenance may be required. Guided Diagnostics, Meter Monitor, and time-stamped system records also support troubleshooting by tracking parameters such as vacuum levels, gas flows, and temperatures.</p><p>Method and batch setup are designed to reduce manual configuration. Batches can be created from preset methods, templates, existing batches, Method Wizard, or Method Advisor, and legacy Agilent ICP-MS MassHunter batches can be opened directly in OpenLab ICP-MS. For the <strong>9500 ICP-QQQ</strong>, Method Advisor provides an element-focused approach in which users select target elements and calibration information while the software applies recommended acquisition masses and cell-gas conditions. Preset methods are available for applications including <strong>EPA 200.8/EPA 6020, USP &lt;232&gt;, ICH Q3D, and Chinese Pharmacopoeia requirements</strong>, while an IntelliQuant Screening preset supports semiquantitative screening of unknown samples. Routine instrument tasks can also be automated through autotuning, startup checks, batch queues, end-of-run verification, rinse functions, and automatic shutdown.</p><p>For data evaluation, OpenLab ICP-MS provides a real-time workspace where users can review analyte concentrations, internal-standard recoveries, stability plots, spectra or chromatograms, calibration information, QC charts, and IntelliQuant results in a single view. <strong>IntelliQuant</strong> acquires a complete mass spectrum and displays semiquantitative elemental concentrations using a color-coded periodic table, while <strong>IntelliQuant Star Rating</strong> assigns a zero-to-five-star data-quality score based on factors such as potential interferences, calibration quality, background, detection limits, and precision. Reporting options include whole-batch reports, elemental impurity reports for USP &lt;232&gt;/&lt;233&gt; and ICH Q3D, customizable reports, structured CSV export, and direct data transfer to LIMS.</p><p>The software can be expanded for specialized applications, including <strong>LC-ICP-MS and GC-ICP-MS</strong>, advanced QC workflows, single-particle ICP-MS and FFF-ICP-MS, ADS 2 automation, semiconductor analysis, and peripheral-device control. Supported analytical approaches include external calibration, standard additions, semiquantitative calibration, isotope ratios, and isotope dilution. For regulated laboratories, OpenLab ICP-MS can be combined with scalable OpenLab compliance solutions providing electronic signatures, user access control, configurable roles, system activity logs, and audit trails, supporting workflows subject to <strong>21 CFR Part 11, EU Annex 11, and equivalent regulations</strong>. Overall, the platform is positioned as a unified environment for routine and advanced ICP-MS workflows, combining instrument control, method setup, diagnostics, data-quality assessment, reporting, and compliance support.</p><h3><strong>2. Shimadzu: Identification of Virgin PET and Recycled PET by X-ray Fluorescence Spectrometry</strong></h3><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/pdf/an_01_01204_en_f3f20ff020.pdf"><strong>Full PDF for download</strong></a></li></ul><h5><strong>User benefits</strong></h5><ul><li>EDX enables the identification of recycled PET.&nbsp;</li><li>Measurements are quick and simple, require no cumbersome pretreatment, and can be automated using a multi-sample turret.&nbsp;</li><li>The instrument offers excellent cost-performance and supports the detection of a wide range of elements.</li></ul><p>Establishing a sustainable circular economy is a major societal challenge, and recycling plastic materials such as PET (polyethylene terephthalate) plays a particularly important role in reducing environmental impact. Large numbers of PET bottles and molded products are used every day in the food and beverage sectors. To recycle these materials safely and reliably, technologies are required that can accurately identify their origin. In practice, however, appearance and conventional physical properties alone are insufficient to distinguish virgin material from recycled material, creating a need for a more reliable identification method.&nbsp;</p><p>For rapid identification in industrial settings, a method requiring little or no pretreatment is highly desirable. In some cases, nondestructive analysis is also needed to enable subsequent application of other analytical techniques. This article presents a practical approach in which metal catalysts present in PET are detected by EDX (Energy-Dispersive X-ray Spectroscopy) and used to distinguish material-recycled PET from virgin PET.</p><h4><strong>Principle and Overview&nbsp;</strong></h4><p>Metal catalysts such as antimony (Sb) and germanium (Ge) are used in the synthesis of PET resin. These catalyst metals have been reported to be useful indicators of material origin. 1),2) For example, Sb and Ge are frequently detected together in material-recycled PET, whereas only one catalyst metal is detected in chemically recycled PET and virgin PET. This likely reflects the fact that material-recycled PET is derived from a mixture of feedstocks using different catalysts.&nbsp;</p><p>ICP-AES (ICP optical emission spectrometry) and ICP-MS (ICP mass spectrometry), which are commonly applied to catalyst metal analysis, provide high sensitivity and accuracy. However, they require pretreatment to convert the sample into a solution, thereby lengthening the analytical workflow. By contrast, EDX can measure solid samples directly, making it well-suited to applications requiring rapid results, such as incoming material inspection and in-line analysis in molding plants. Because EDX is non-destructive, it is also suitable for multimodal analytical workflows.&nbsp;</p><p>On the other hand, some commercially available handheld EDX instruments do not support elements such as Sb and Ge. At the same time, higher-end systems may not offer the specifications or price range needed for industrial deployment. The <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/icpms/library?mainauthorItems=1&amp;search=EDX-7200"><strong>EDX-7200</strong></a> supports a broad range of elements with excellent cost performance. This article describes the analysis of Sb and Ge in PET using this instrument.</p><h4><strong>Conclusion&nbsp;</strong></h4><p>EDX enables rapid and straightforward elemental analysis without cumbersome sample pretreatment. Previous studies have shown that the presence of Sb and Ge can be used to identify recycled PET. Building on this concept, this article presents a practical analytical approach based on EDX. Using the EDX-7200, which combines broad elemental coverage with excellent cost performance, the proposed method provides a practical tool for rapid on-site identification, quality control, and traceability management. When combined with physical property data and other information, this approach is expected to contribute to the safety assessment and quality assurance of recycled materials, thereby supporting a more advanced circular economy.</p><h3><strong>3. Thermo Fisher Scientific: Optimizing lithium-ion battery recycling operations using handheld XRF analysis</strong></h3><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/pdf/lithium_ion_battery_recycling_handheld_xrf_analysis_an1120_en_4c00477b78.pdf"><strong>Full PDF for download</strong></a></li></ul><p>The shift to a low-carbon economy and the adoption of electric vehicles will drive an exponential increase in the demand for lithium-ion batteries. As a corollary to this, the International Energy Agency expects the demand for some key commodities to increase significantly over the next two decades: the demand for Copper (Cu) is anticipated to increase by more than 40%; for nickel (Ni) and cobalt (Co), by 60-70% each; and for lithium (Li), by nearly 90%.¹ This will translate into increased mining activities and potentially generate larger amounts of deleterious waste.&nbsp;</p><p>To reduce the environmental impact and limit reliance on scarce commodities associated with economical and geopolitical implications, several countries have implemented regulations regarding producers’ responsibilities.² These regulations contain both incentives and accountability guidelines for lithium-ion battery and electric vehicles manufacturers. Their goal is to facilitate the emergence of a circular economy in which recycling will increasingly contribute to the supply of the strategic raw materials.&nbsp;</p><p>Lithium-ion batteries are made of multiple components, the most valuable being the cathode that contains between 40 and 70% ³, ⁴ of the total value of the battery, depending on its exact chemistry. As of 2023, lithium nickel cobalt manganese oxides (NCM) account for 66% of lithium-ion battery cathode active materials for electric vehicles, followed by lithium iron phosphates (LFP) which account for 24%, and lithium nickel cobalt aluminum oxide (NCA) accounts for the remaining 10%.³</p><h4><strong>Handheld X-ray Fluorescence Analysis&nbsp;</strong></h4><p>Handheld X-ray fluorescence analysis (HHXRF) is an elemental analysis technique that has proven to be cost-effective in recycling areas such as scrap metal and automotive catalytic converters. HHXRF can measure elements from magnesium (Mg) to uranium (U) in various types of materials such as metals and alloys; non-metallic inorganic materials such as ceramics; or ores or plastics. The <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/1993"><strong>Thermo Scientific™ Niton™ XL2</strong></a> and <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/1992"><strong>Thermo Scientific™ Niton™ XL5 Plus Handheld XRF Analyzers </strong></a>deliver accurate elemental analysis in real time, with little or no sample preparation, across multiple steps of the lithium-ion battery recycling workflow. Although handheld XRF does not detect lithium, it can measure most elements from the periodic table including nickel or cobalt which often command much higher value than the lithium in a lithium-ion battery.⁴</p><h4><strong>Conclusion&nbsp;</strong></h4><p>There is no ideal process to recycle lithium-ion batteries that simultaneously incorporates low environmental impact, high metal recovery yield, and economic viability. Because of the variety of technologies and materials used, recycling lithium-ion batteries is a complex journey with multiple possible paths. HHXRF helps recyclers by generating lab-quality data in real time, allowing them to optimize their processes and make fast decisions that generate significant benefits:&nbsp;</p><ul><li>Unwanted materials containing heavy metals such as lead or cadmium can be prevented from entering subsequent steps in the recycling workflow.&nbsp;</li><li>Materials can be accurately sorted and adequate processes for recovery selected depending on the material type (e.g., LFP vs. MCM).&nbsp;</li><li>The economic value of incoming and outgoing material can be more accurately estimated.</li></ul><h3><strong>4. Waters Corporation: Waters Aura Systems</strong></h3><ul><li>Brochure</li><li><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/pdf/720009268_7b9ad02cb4.pdf"><strong>Full PDF for download</strong></a></li></ul><p>The presentation introduces the <strong>Waters Aura Systems</strong>, a family of high-throughput, fluidics-free instruments for the characterization and identification of visible and subvisible particles. All Aura platforms provide particle counting, identification, morphology assessment, and flexible sample volumes ranging from microliters to milliliters. The portfolio includes configurations tailored to different applications: <strong>AuraBMI</strong> for biologics particle analysis, <strong>Aura</strong> for particle analysis with identification, <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/2437"><strong>AuraPTx</strong></a> for protein formulation development, <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/2438"><strong>AuraGT</strong></a> for gene therapy, <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/2439"><strong>AuraCL</strong></a> for cell therapy, and <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/2190"><strong>Aura+</strong></a> as the most comprehensive platform. The systems are designed for automation-ready operation, straightforward method transfer, and continuity from research through QC.</p><p>A key feature of the Aura platform is the combination of <strong>Backgrounded Membrane Imaging (BMI), Fluorescence Membrane Microscopy (FMM), and Side Illumination Membrane Imaging (SIMI)</strong>. BMI captures particles on a membrane and subtracts the membrane background to improve particle contrast, while FMM uses fluorescent dyes or conjugated antibodies to distinguish specific particle types. This enables differentiation of protein aggregates, cells, viral capsids, degraded excipients, plastics, fibers, and other contaminants that may look similar based on morphology alone. SIMI adds further information for identifying unlabeled inorganic particles such as glass, fibers, and Dynabeads. Together, these techniques provide more specific particle identification than morphology-based classification alone.</p><p>The systems are particularly suited to <strong>biologics, gene therapy, and cell therapy development</strong>. For gene therapy, Aura can evaluate AAV stability, distinguish capsid-related particles, and monitor DNA leakage using SYBR Gold fluorescence, with measurements possible from as little as <strong>5 µL of sample</strong>. For cell therapy, the system can differentiate single cells, cell aggregates, protein aggregates, and extrinsic particles. The platform also supports flexible sample volumes and 24- or 96-well membrane formats, allowing the same general approach to be used from sample-limited early development through larger-volume and QC workflows. The brochure reports excellent quantitative linearity across serial dilutions and emphasizes the ability to preserve sample for additional orthogonal analyses.</p><p>From a technical perspective, Aura Systems provide <strong>100% sampling efficiency</strong>, a particle detection and quantitation range above <strong>1 µm</strong>, and can handle concentrations above <strong>3,000,000 particles/mL</strong> for 1.6 µm particles. Brightfield membrane imaging takes approximately <strong>one minute per sample</strong>, while fluorescence measurements require about <strong>15–30 seconds per sample</strong>. The instruments are compatible with robotic automation and offer different fluorescence-channel configurations depending on the selected Aura model. Overall, the platform is positioned as a comprehensive solution for obtaining quantitative particle counts together with information on particle identity and composition across the development and quality-control lifecycle.</p>

News from LabRulezICPMS Library - Week 36, 2026

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The Czech Academy of Sciences (CAS) was established by Act No. 283/1992 Coll. as the Czech successor of the former Czechoslovak Academy of Sciences. It is set up as a complex of 54 public research institutions.

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Organomation, founded in 1959, designs and manufactures high-quality nitrogen evaporators and extraction systems. Known for innovation and durability, their lab instruments are used globally for efficient sample preparation with strong customer support.

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Thermo Scientific FlashSmart Elemental Analyzer CHNS/O

The Thermo Scientific™ FlashSmart™ Elemental Analyzer (EA), based on the modified Dumas Method, is a flexible solution that expands your CHNS/O analysis with over 20 configurations in one system.

<h3><strong>Lead the way in elemental analysis with a single instrument handling all applications.</strong></h3><p>You and your team can solve more laboratory challenges, improve workflow and minimize downtime. The <strong>Thermo Scientific™ FlashSmart™ Elemental Analyzer </strong>(EA), based on the <strong>modified Dumas Method</strong>, is a flexible solution that expands your <strong>CHNS/O</strong> analysis with <strong>over 20 configurations</strong> <strong>in one system</strong>. Powerful software supports automated and precise reports, making everything easier for you and your team.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_Flash_Smart_Elemental_Analyzer_CHNS_O_2_efeac51a98.jpg" alt="Thermo Scientific™ FlashSmart™ Elemental Analyzer CHNS/O" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_Flash_Smart_Elemental_Analyzer_CHNS_O_2_efeac51a98.jpg 245w," sizes="100vw" width="1424" height="888"></p><h3><strong>Why choose the FlashSmart EA?</strong></h3><h4><strong>The confident choice</strong></h4><ul><li><strong>Precise and reliable</strong> system that delivers accurate results</li><li><strong>Easy maintenance</strong></li><li><strong>Easy to use </strong>for reduced need for staff training</li><li>Modern design combines simple user input with <strong>dedicated software features</strong></li><li><strong>Better return on investment </strong>as the system is modular and grows with your analytical requirements</li></ul><h4><strong>Simple</strong></h4><ul><li><strong>Gas chromatographic method for real-time view of the analytical process and pathway:</strong> anytime, anywhere</li><li><strong>Streamlined sample preparation </strong>without the need for dangerous chemicals as Kjeldahl Method</li><li><strong>Complete EA software</strong> for effortless operation</li></ul><h4><strong>Modular</strong></h4><ul><li><strong>Over 20 configurations in one instrument:</strong> no need for software upgrade</li><li><strong>Up to two autosamplers </strong>on the same analyzer</li><li>Higher sample throughput and automation with the <strong>Thermo Scientific™ MultiValve Control (MVC) Module</strong>, without manual intervention</li><li>Operates with <strong>helium</strong> and <strong>argon </strong>as carrier gas</li></ul><h4><strong>Automated</strong></h4><ul><li><strong>Unattended operation</strong> of the FlashSmart EA: analyses can run <strong>24/7</strong> for complete results anytime, anywhere</li><li>Dedicated <strong>Thermo Scientific™ EagerSmart™ </strong>Data</li><li>Handling Software controlling all analytical parameters, Thermo <strong>Scientific™ OxyTune™ Function</strong>, an autosampler and the MVC Module</li><li><strong>Lower cost </strong>per analysis and greater productivity</li></ul><h4><strong>Accurate</strong></h4><ul><li><strong>Certified </strong>and uncompromised precision and accuracy for a wide range of applications, from research to routine analysis</li><li><strong>Compliance with most recognized EA Official Methods: </strong>AOAC, AOCS, AACC, ASTM, ASBC, ISO, EN, CEN, EPA, IFFO</li><li><strong>OEA CookBook</strong> with <strong>thousands</strong> of determinations and methods for optimal results</li></ul><h4><strong>Robust</strong></h4><ul><li>Robust, specially designed features that you can rely on for decades</li><li><strong>GC separation column operating for years without the need for replacement: </strong>it is not a consumable</li><li>Long term investment for your laboratory, which guarantees<strong> reliability and accuracy</strong> of analysis</li></ul><h3><strong>Access more applications: become the reference laboratory in your field</strong></h3><p>No matter which direction you take, your lab and equipment will be able to adapt to support any strategy. Flexible systems enable you to react to the new, whilst delivering accurate and reproducible results. With the <strong>FlashSmart EA</strong> your lab can easily handle varying sample types, obtain from 1 to 5 element determinations and achieve maximum sample throughput.</p><h4><strong>CHNS/O Analyzer Configuration</strong></h4><ul><li><strong>Perform 5 elements analysis with TCD</strong></li><li><strong>Organic Chemistry: </strong>organo-metallic compounds, polymers, plastic, synthetic rubbers, fibers, explosives, catalysts, textiles, pesticides, detergents, and fluorine-compounds.</li><li><strong>Petro-chemistry &amp; Energy: </strong>Coals, cokes, crude oils, alternative fuels, petroleum derivates, lubricants, oil additives, and graphite.</li><li><strong>Environmental: </strong>Soils, sediments, and rocks, composts, wastes, sewage/sludge, pesticides, water solution, waste water, particulates in air by filters, particulates in water by filters, and woods.</li><li><strong>Material Characterization: </strong>Battery, glue/resins, papers, rubbers, cement, ceramics, carbon/glass fibers, tires, pigments and dyes, refractory materials, building materials, inorganic materials, metals, textile fibers, and wood powders.</li></ul><h3><strong>Performance that takes you further</strong></h3><p>With powerful yet easy operation, your team can process <strong>more samples every day</strong>. When you need to analyze more elements, you can adapt the <strong>FlashSmart EA on-site </strong>to your applications or <strong>add a second reactor</strong> to unlock more capabilities.</p><h4><strong>Instantly connect</strong></h4><ul><li>Thermal Conductivity Detector (TCD)</li></ul><h4><strong>Sample introduction modularity</strong></h4><ul><li>Up to <strong>two Thermo Scientific™ MAS Plus Autosamplers</strong></li><li>One MAS Plus Autosampler and one manual liquid sampler</li></ul><h4><strong>Carrier gas options</strong></h4><ul><li>Helium</li><li>Argon option for lower cost and regular supply</li><li>Switch to nitrogen or argon when in Stand-By Mode</li></ul><h4><strong>Gas chromatographic method: real-time analysis</strong></h4><ul><li>Proper quantification of the <strong>five elements</strong></li><li><strong>“Open window” </strong>function giving information on what is happening inside the analyzer in real-time</li><li>Straightforward and intuitive workflow without valves</li><li>No absorption or desorption of gases needed</li></ul><figure class="image"><img style="aspect-ratio:1482/903;" src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_Flash_Smart_Elemental_Analyzer_CHNS_O_3_ae03e912c7.jpg" alt="Thermo Scientific™ FlashSmart™ Elemental Analyzer CHNS/O" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_Flash_Smart_Elemental_Analyzer_CHNS_O_3_ae03e912c7.jpg 245w," sizes="100vw" width="1482" height="903"></figure><h3><strong>Software automates consistent sampling and reports</strong></h3><h4><strong>Software</strong></h4><p>The <strong>Thermo Scientific EagerSmart Data Handling Software</strong> allows you to leave the <strong>FlashSmart EA </strong>unattended to get completed analysis, with full, user-friendly reports. The software controls all analytical parameters, flows, autosamplers and detectors, by suggesting the most favourable analytical conditions for your samples.</p><ul><li><strong>Automated transfer</strong> <strong>of the sample</strong> weight from the balance to the software</li><li><strong>Automated evaluation of Heat Values</strong> (Gross and Net Heat Values) for fuels and alternative fuels</li><li><strong>CO2 Emission Trade</strong> for environmental control</li><li><strong>Different Protein Factors</strong> for food and animal feed</li><li><strong>Inserting of the Humidity value</strong> for solid samples and of the Density for liquid samples</li><li><strong>Automated Minimal Formula determination </strong>for pharmaceutical or fine chemicals applications</li><li><strong>Automated evaluation of C/N, C/H and C/S ratio</strong></li><li><strong>Automated data transfer</strong> to Microsoft Excel, LIMS and others</li></ul><h4><strong>Automated functions</strong></h4><ul><li>Auto-Start</li><li>Auto-Ready</li><li>Auto-Stand-By</li><li>Auto-Off</li><li>Auto Leak Test</li></ul><h4><strong>Unique and dedicated OxyTune function</strong></h4><p>The Thermo Scientific <strong>OxyTune Function</strong> automatically evaluates the oxygen needed for combustion, according to the weight and nature of your sample.</p><h4><strong>MultiValve Control Module: future-proof lab with more throughput and less costs</strong></h4><p>By switching the analysis from the left channel to the right one (or viceversa), the MVC Module increases your analysis throughput. When the system is not in use overnight, on weekends, or for a prolonged period of time you can also reduce helium consumption and overall cost of analysis by switching from helium to nitrogen or argon.</p><ul><li>Fully automated and software controlled</li><li>No need to change hardware or software configuration</li><li>Optional feature for extended lab throughput</li><li>Easy to add</li></ul>

Thermo Scientific™ FlashSmart™ Elemental Analyzer NC/Soil

<h3><strong>Lead the way in elemental analysis with a single instrument handling all applications.</strong></h3><p>You and your team can solve more laboratory challenges, improve workflow and minimize downtime. The <strong>Thermo Scientific™ FlashSmart™ Elemental Analyzer </strong>(EA), based on the <strong>modified Dumas Method</strong>, is a flexible solution that expands your <strong>CHNS/O</strong> analysis with <strong>over 20 configurations</strong> <strong>in one system</strong>. Powerful software supports automated and precise reports, making everything easier for you and your team.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_Flash_Smart_Elemental_Analyzer_CHNS_O_2_efeac51a98.jpg" alt="Thermo Scientific™ FlashSmart™ Elemental Analyzer NC/Soil" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_Flash_Smart_Elemental_Analyzer_CHNS_O_2_efeac51a98.jpg 245w," sizes="100vw" width="1424" height="888"></p><h3><strong>Why choose the FlashSmart EA?</strong></h3><h4><strong>The confident choice</strong></h4><ul><li><strong>Precise and reliable</strong> system that delivers accurate results</li><li><strong>Easy maintenance</strong></li><li><strong>Easy to use </strong>for reduced need for staff training</li><li>Modern design combines simple user input with <strong>dedicated software features</strong></li><li><strong>Better return on investment </strong>as the system is modular and grows with your analytical requirements</li></ul><h4><strong>Simple</strong></h4><ul><li><strong>Gas chromatographic method for real-time view of the analytical process and pathway:</strong> anytime, anywhere</li><li><strong>Streamlined sample preparation </strong>without the need for dangerous chemicals as Kjeldahl Method</li><li><strong>Complete EA software</strong> for effortless operation</li></ul><h4><strong>Modular</strong></h4><ul><li><strong>Over 20 configurations in one instrument:</strong> no need for software upgrade</li><li><strong>Up to two autosamplers </strong>on the same analyzer</li><li>Higher sample throughput and automation with the <strong>Thermo Scientific™ MultiValve Control (MVC) Module</strong>, without manual intervention</li><li>Operates with <strong>helium</strong> and <strong>argon </strong>as carrier gas</li></ul><h4><strong>Automated</strong></h4><ul><li><strong>Unattended operation</strong> of the FlashSmart EA: analyses can run <strong>24/7</strong> for complete results anytime, anywhere</li><li>Dedicated <strong>Thermo Scientific™ EagerSmart™ </strong>Data</li><li>Handling Software controlling all analytical parameters, Thermo <strong>Scientific™ OxyTune™ Function</strong>, an autosampler and the MVC Module</li><li><strong>Lower cost </strong>per analysis and greater productivity</li></ul><h4><strong>Accurate</strong></h4><ul><li><strong>Certified </strong>and uncompromised precision and accuracy for a wide range of applications, from research to routine analysis</li><li><strong>Compliance with most recognized EA Official Methods: </strong>AOAC, AOCS, AACC, ASTM, ASBC, ISO, EN, CEN, EPA, IFFO</li><li><strong>OEA CookBook</strong> with <strong>thousands</strong> of determinations and methods for optimal results</li></ul><h4><strong>Robust</strong></h4><ul><li>Robust, specially designed features that you can rely on for decades</li><li><strong>GC separation column operating for years without the need for replacement: </strong>it is not a consumable</li><li>Long term investment for your laboratory, which guarantees<strong> reliability and accuracy</strong> of analysis</li></ul><h3><strong>Access more applications: become the reference laboratory in your field</strong></h3><p>No matter which direction you take, your lab and equipment will be able to adapt to support any strategy. Flexible systems enable you to react to the new, whilst delivering accurate and reproducible results. With the <strong>FlashSmart EA</strong> your lab can easily handle varying sample types, obtain from 1 to 5 element determinations and achieve maximum sample throughput.</p><h4><strong>NC Soil Configuration</strong></h4><ul><li><strong>Determination of Total Nitrogen, Total Carbon, and Total Organic Carbon.</strong></li><li><strong>Environmental: </strong>Soils, sediments, and rocks, composts, wastes, sewage/sludge, pesticides, water solution, waste water, particulates in air by filters, particulates in water by filters, and woods.</li><li><strong>Material Characterization: </strong>Battery, glue/resins, papers, rubbers, cement, ceramics, carbon/glass fibers, tires, pigments and dyes, refractory materials, building materials, inorganic materials, metals, textile fibers, and wood powders.</li><li><strong>Agronomy &amp; Marine Science: </strong>Soil, plants (leaves, roots, fruit), sediments, humus, algae, plankton, particulate matter in water by filters, water, and fertilizer.</li></ul><h3><strong>Performance that takes you further</strong></h3><p>With powerful yet easy operation, your team can process <strong>more samples every day</strong>. When you need to analyze more elements, you can adapt the <strong>FlashSmart EA on-site </strong>to your applications or <strong>add a second reactor</strong> to unlock more capabilities.</p><h4><strong>Instantly connect</strong></h4><ul><li>Thermal Conductivity Detector (TCD)</li></ul><h4><strong>Sample introduction modularity</strong></h4><ul><li>Up to <strong>two Thermo Scientific™ MAS Plus Autosamplers</strong></li><li>One MAS Plus Autosampler and one manual liquid sampler</li></ul><h4><strong>Carrier gas options</strong></h4><ul><li>Helium</li><li>Argon option for lower cost and regular supply</li><li>Switch to nitrogen or argon when in Stand-By Mode</li></ul><h4><strong>Gas chromatographic method: real-time analysis</strong></h4><ul><li>Proper quantification of the <strong>five elements</strong></li><li><strong>“Open window” </strong>function giving information on what is happening inside the analyzer in real-time</li><li>Straightforward and intuitive workflow without valves</li><li>No absorption or desorption of gases needed</li></ul><figure class="image"><img style="aspect-ratio:1482/903;" src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_Flash_Smart_Elemental_Analyzer_CHNS_O_3_ae03e912c7.jpg" alt="Thermo Scientific™ FlashSmart™ Elemental Analyzer NC/Soil" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_Flash_Smart_Elemental_Analyzer_CHNS_O_3_ae03e912c7.jpg 245w," sizes="100vw" width="1482" height="903"></figure><h3><strong>Software automates consistent sampling and reports</strong></h3><h4><strong>Software</strong></h4><p>The <strong>Thermo Scientific EagerSmart Data Handling Software</strong> allows you to leave the <strong>FlashSmart EA </strong>unattended to get completed analysis, with full, user-friendly reports. The software controls all analytical parameters, flows, autosamplers and detectors, by suggesting the most favourable analytical conditions for your samples.</p><ul><li><strong>Automated transfer</strong> <strong>of the sample</strong> weight from the balance to the software</li><li><strong>Automated evaluation of Heat Values</strong> (Gross and Net Heat Values) for fuels and alternative fuels</li><li><strong>CO2 Emission Trade</strong> for environmental control</li><li><strong>Different Protein Factors</strong> for food and animal feed</li><li><strong>Inserting of the Humidity value</strong> for solid samples and of the Density for liquid samples</li><li><strong>Automated Minimal Formula determination </strong>for pharmaceutical or fine chemicals applications</li><li><strong>Automated evaluation of C/N, C/H and C/S ratio</strong></li><li><strong>Automated data transfer</strong> to Microsoft Excel, LIMS and others</li></ul><h4><strong>Automated functions</strong></h4><ul><li>Auto-Start</li><li>Auto-Ready</li><li>Auto-Stand-By</li><li>Auto-Off</li><li>Auto Leak Test</li></ul><h4><strong>Unique and dedicated OxyTune function</strong></h4><p>The Thermo Scientific <strong>OxyTune Function</strong> automatically evaluates the oxygen needed for combustion, according to the weight and nature of your sample.</p><h4><strong>MultiValve Control Module: future-proof lab with more throughput and less costs</strong></h4><p>By switching the analysis from the left channel to the right one (or viceversa), the MVC Module increases your analysis throughput. When the system is not in use overnight, on weekends, or for a prolonged period of time you can also reduce helium consumption and overall cost of analysis by switching from helium to nitrogen or argon.</p><ul><li>Fully automated and software controlled</li><li>No need to change hardware or software configuration</li><li>Optional feature for extended lab throughput</li><li>Easy to add</li></ul>

Thermo Scientific™ FlashSmart™ Elemental Analyzer N/Protein

<h3><strong>Lead the way in elemental analysis with a single instrument handling all applications.</strong></h3><p>You and your team can solve more laboratory challenges, improve workflow and minimize downtime. The <strong>Thermo Scientific™ FlashSmart™ Elemental Analyzer </strong>(EA), based on the <strong>modified Dumas Method</strong>, is a flexible solution that expands your <strong>CHNS/O</strong> analysis with <strong>over 20 configurations</strong> <strong>in one system</strong>. Powerful software supports automated and precise reports, making everything easier for you and your team.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_Flash_Smart_Elemental_Analyzer_CHNS_O_2_efeac51a98.jpg" alt="Thermo Scientific™ FlashSmart™ Elemental Analyzer N/Protein" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_Flash_Smart_Elemental_Analyzer_CHNS_O_2_efeac51a98.jpg 245w," sizes="100vw" width="1424" height="888"></p><h3><strong>Why choose the FlashSmart EA?</strong></h3><h4><strong>The confident choice</strong></h4><ul><li><strong>Precise and reliable</strong> system that delivers accurate results</li><li><strong>Easy maintenance</strong></li><li><strong>Easy to use </strong>for reduced need for staff training</li><li>Modern design combines simple user input with <strong>dedicated software features</strong></li><li><strong>Better return on investment </strong>as the system is modular and grows with your analytical requirements</li></ul><h4><strong>Simple</strong></h4><ul><li><strong>Gas chromatographic method for real-time view of the analytical process and pathway:</strong> anytime, anywhere</li><li><strong>Streamlined sample preparation </strong>without the need for dangerous chemicals as Kjeldahl Method</li><li><strong>Complete EA software</strong> for effortless operation</li></ul><h4><strong>Modular</strong></h4><ul><li><strong>Over 20 configurations in one instrument:</strong> no need for software upgrade</li><li><strong>Up to two autosamplers </strong>on the same analyzer</li><li>Higher sample throughput and automation with the <strong>Thermo Scientific™ MultiValve Control (MVC) Module</strong>, without manual intervention</li><li>Operates with <strong>helium</strong> and <strong>argon </strong>as carrier gas</li></ul><h4><strong>Automated</strong></h4><ul><li><strong>Unattended operation</strong> of the FlashSmart EA: analyses can run <strong>24/7</strong> for complete results anytime, anywhere</li><li>Dedicated <strong>Thermo Scientific™ EagerSmart™ </strong>Data</li><li>Handling Software controlling all analytical parameters, Thermo <strong>Scientific™ OxyTune™ Function</strong>, an autosampler and the MVC Module</li><li><strong>Lower cost </strong>per analysis and greater productivity</li></ul><h4><strong>Accurate</strong></h4><ul><li><strong>Certified </strong>and uncompromised precision and accuracy for a wide range of applications, from research to routine analysis</li><li><strong>Compliance with most recognized EA Official Methods: </strong>AOAC, AOCS, AACC, ASTM, ASBC, ISO, EN, CEN, EPA, IFFO</li><li><strong>OEA CookBook</strong> with <strong>thousands</strong> of determinations and methods for optimal results</li></ul><h4><strong>Robust</strong></h4><ul><li>Robust, specially designed features that you can rely on for decades</li><li><strong>GC separation column operating for years without the need for replacement: </strong>it is not a consumable</li><li>Long term investment for your laboratory, which guarantees<strong> reliability and accuracy</strong> of analysis</li></ul><h3><strong>Access more applications: become the reference laboratory in your field</strong></h3><p>No matter which direction you take, your lab and equipment will be able to adapt to support any strategy. Flexible systems enable you to react to the new, whilst delivering accurate and reproducible results. With the <strong>FlashSmart EA</strong> your lab can easily handle varying sample types, obtain from 1 to 5 element determinations and achieve maximum sample throughput.</p><h4><strong>N/Protein Analyzer Configuration</strong></h4><ul><li><strong>Determine crude protein in human food and animal feed using quality certified Reference Material, included as standard.</strong></li><li><strong>Food Safety: </strong>Human food and animal feed, beverages (beer, juice, milk, wine, soft drinks...).</li></ul><h3><strong>Performance that takes you further</strong></h3><p>With powerful yet easy operation, your team can process <strong>more samples every day</strong>. When you need to analyze more elements, you can adapt the <strong>FlashSmart EA on-site </strong>to your applications or <strong>add a second reactor</strong> to unlock more capabilities.</p><h4><strong>Instantly connect</strong></h4><ul><li>Thermal Conductivity Detector (TCD)</li></ul><h4><strong>Sample introduction modularity</strong></h4><ul><li>Up to <strong>two Thermo Scientific™ MAS Plus Autosamplers</strong></li><li>One MAS Plus Autosampler and one manual liquid sampler</li></ul><h4><strong>Carrier gas options</strong></h4><ul><li>Helium</li><li>Argon option for lower cost and regular supply</li><li>Switch to nitrogen or argon when in Stand-By Mode</li></ul><h4><strong>Gas chromatographic method: real-time analysis</strong></h4><ul><li>Proper quantification of the <strong>five elements</strong></li><li><strong>“Open window” </strong>function giving information on what is happening inside the analyzer in real-time</li><li>Straightforward and intuitive workflow without valves</li><li>No absorption or desorption of gases needed</li></ul><figure class="image"><img style="aspect-ratio:1482/903;" src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_Flash_Smart_Elemental_Analyzer_CHNS_O_3_ae03e912c7.jpg" alt="Thermo Scientific™ FlashSmart™ Elemental Analyzer N/Protein" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_Flash_Smart_Elemental_Analyzer_CHNS_O_3_ae03e912c7.jpg 245w," sizes="100vw" width="1482" height="903"></figure><h3><strong>Software automates consistent sampling and reports</strong></h3><h4><strong>Software</strong></h4><p>The <strong>Thermo Scientific EagerSmart Data Handling Software</strong> allows you to leave the <strong>FlashSmart EA </strong>unattended to get completed analysis, with full, user-friendly reports. The software controls all analytical parameters, flows, autosamplers and detectors, by suggesting the most favourable analytical conditions for your samples.</p><ul><li><strong>Automated transfer</strong> <strong>of the sample</strong> weight from the balance to the software</li><li><strong>Automated evaluation of Heat Values</strong> (Gross and Net Heat Values) for fuels and alternative fuels</li><li><strong>CO2 Emission Trade</strong> for environmental control</li><li><strong>Different Protein Factors</strong> for food and animal feed</li><li><strong>Inserting of the Humidity value</strong> for solid samples and of the Density for liquid samples</li><li><strong>Automated Minimal Formula determination </strong>for pharmaceutical or fine chemicals applications</li><li><strong>Automated evaluation of C/N, C/H and C/S ratio</strong></li><li><strong>Automated data transfer</strong> to Microsoft Excel, LIMS and others</li></ul><h4><strong>Automated functions</strong></h4><ul><li>Auto-Start</li><li>Auto-Ready</li><li>Auto-Stand-By</li><li>Auto-Off</li><li>Auto Leak Test</li></ul><h4><strong>Unique and dedicated OxyTune function</strong></h4><p>The Thermo Scientific <strong>OxyTune Function</strong> automatically evaluates the oxygen needed for combustion, according to the weight and nature of your sample.</p><h4><strong>MultiValve Control Module: future-proof lab with more throughput and less costs</strong></h4><p>By switching the analysis from the left channel to the right one (or viceversa), the MVC Module increases your analysis throughput. When the system is not in use overnight, on weekends, or for a prolonged period of time you can also reduce helium consumption and overall cost of analysis by switching from helium to nitrogen or argon.</p><ul><li>Fully automated and software controlled</li><li>No need to change hardware or software configuration</li><li>Optional feature for extended lab throughput</li><li>Easy to add</li></ul>

Thermo Scientific™ EA IsoLink™ IRMS System

With the Thermo Scientific™ EA IsoLink™ IRMS Platform, leverage familiar technology and existing expertise for expanded CNSOH isotope analysis, allowing all elemental analysis on a single platform.

<h3><strong>All your elemental analysis on one platform</strong></h3><p><strong>The EA IsoLink IRMS Platform leverages the existing technological platform of the EA IsoLink IRMS System and FlashSmart EA.</strong></p><h4><strong>More freedom. More flexibility.</strong></h4><p>With the<strong> Thermo Scientific™ EA IsoLink™ IRMS Platform</strong>, you can leverage familiar technology and your staff’s existing know-how for <strong>expanded CNSOH isotope analysis</strong>, enabling you to perform all your elemental analysis on one technological platform. With <strong>different configurations</strong> to choose from, your lab can get the capabilities it needs today, with flexibility for the future. Featuring software- driven automation and scalability to grow as you do.</p><h4><strong>Choose the configuration that’s right for you.</strong></h4><p>The<strong> EA IsoLink IRMS</strong> System is an automated, easy-to-use solution for <strong>isotopic analysis of carbon, nitrogen, sulfur, oxygen and hydrogen</strong> - using bulk samples powered by chromatography-driven technology with high sensitivity on small samples. Available in basic configurations with upgradeability options, this platform offers high throughput and unattended operation, so your lab can get more done in less time.</p><h4><strong>The EA IsoLink IRMS System features:</strong></h4><ul><li><strong>Thermo Scientific™ Flash™ IRMS EA</strong> for sample preparation for IRMS analysis</li><li><a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/2231"><strong>Thermo Scientific™ ConFlo IV</strong></a> Universal Interface</li><li><a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/2232"><strong>Thermo Scientific™ DELTA™ Q IRMS</strong></a></li></ul><h4><strong>The FlashSmart EA features:</strong></h4><ul><li><strong>Thermo Scientific™ FlashSmart™ EA</strong> for weight percentage characterization of CNSHO</li></ul><h3><strong>EA IsoLink CN and CN/OH</strong></h3><ul><li>A powerful solution for <strong>C and N, O and H analysis</strong> - upgradeable for <strong>S analysis</strong></li></ul><h3><strong>EA IsoLink OH</strong></h3><ul><li>Offering dedicated<strong> oxygen and hydrogen analysis </strong>- with scalability to expand your capabilities to <strong>C, N and S</strong></li></ul><h3><strong>EA IsoLink CNSOH</strong></h3><ul><li>A fully automated single system for <strong>C, N and S analysis </strong>by flash combustion, and <strong>O and H analysis</strong> by high temperature conversion</li></ul><h4><strong>Connectivity with Thermo Scientific™ IRMS Portfolio</strong></h4><p>The <strong>Flash EA Series</strong> connected to the <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/2232"><strong>DELTA Q IRMS</strong></a><strong> </strong>provides precise and sensitive measurement of the isotope fingerprints - <strong>C, N, S, O and H isotopes </strong>- a unique chemical signature of samples. This helps you gain unique insights into food history and origin, as well as environmental pollutants, forensics and geosciences.</p><figure class="image"><img style="aspect-ratio:650/552;" src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_EA_Iso_Link_IRMS_System_2_01d3ed421c.jpg" alt="Thermo Scientific™ EA IsoLink™ IRMS System" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_EA_Iso_Link_IRMS_System_2_01d3ed421c.jpg 184w," sizes="100vw" width="650" height="552"></figure><h3><strong>More automation. More scalability. All in a single platform.</strong></h3><p><strong>Delivering proven performance with unprecedented robustness and ease of use, the EA IsoLink IRMS Platform can help your lab drive efficiency, improve cost-effectiveness, and minimize training for new operators.</strong></p><h4><strong>Low cost per sample for reduced operational costs</strong></h4><p><strong>Less helium consumption:</strong> Helium consumption is reduced by more than 60% for NCS and NC sample analysis, and reduced by more than 30% for OH sample analysis (compared with previous systems).</p><p><strong>Less replication:</strong> Because the EA IsoLink IRMS System measures high and low concentrations in the same sample (wide dynamic range), it reduces the need for replicate analysis (e.g., high carbon and low sulfur, such as in food authenticity or ecology applications).</p><p><strong>High throughput:</strong> Fast analysis provides high sample throughput, resulting in lower cost per sample.</p><h4><strong>High sensitivity driven by chromatography - even for the smallest sample size</strong></h4><p><strong>Temperature-ramped GC:</strong> Equipped with a temperature-ramped GC feature, the EA IsoLink System gives your lab the highest performance on small sample sizes through optimal baseline separation of analyte gases and sharp peak shapes.</p><p><strong>Performance synergies:</strong> The combination of in-line flash combustion technology and temperature-ramped GC separation significantly improves the performance for all your EA-IRMS applications.</p><h4><strong>System modularity for future-proof investment</strong></h4><p>The <strong>EA IsoLink IRMS</strong> System’s modular design provides the highest flexibility for all applications - enabling you to <strong>adapt and scale</strong> to new analyses in the future. Through smart upgrade paths, you can easily modify the system to increase performance and productivity as your needs grow over time. Boost your CN system with an S upgrade or add CNS to your OH isotope fingerprints.</p><p><strong>Thermo Scientific™ MAS Plus Autosampler</strong> provides a 125-position helium-purged sample chamber, low blank autosampler for CNS and OH analysis.</p><p><strong>Thermo Scientific™ AS 1610 Liquid Autosampler</strong> offers a versatile solution for injecting liquid samples.</p><p>Macro reactors enable CNS Analysis of large sample sizes (greater than 60 mg) and higher throughput on standard sample sizes to mg range.</p><h4><strong>Added flexibility with flash EA series</strong></h4><p>The flexibility of the Flash EA Series helps you meet growing analytical needs in<strong> IRMS and Organic Elemental Analysis</strong> (OEA).</p><p>The <strong>FlashSmart Elemental Analyzer</strong> for OEA delivers accuracy and precision with internationally recognized certifications. Its straightforward modular design offers a variety of optimized application configurations, including <strong>CHN, CHNS, S, N/Protein, CN, CNS, CHNS/O and more</strong>. High throughput with <strong>24/7</strong> operation, low cost per sample and optimized helium consumption are all driven by our fully automated dedicated OEA software, Thermo Scientific™ EagerSmart™ Data Handling Software, which can grow with your analytical needs without need for an upgrade.</p><h4><strong>Smart automation for ease of use</strong></h4><p>Because of its <strong>intelligent software</strong> and intuitive design, the EA IsoLink Platform allows operators to leverage familiar technology for higher productivity.</p><p><strong>Software Platform: </strong><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/1489"><strong>The Thermo Scientific™ Qtegra™ Intelligent Scientific Data Solution</strong> </a>(ISDS) Software provides seamless control and automation for unattended operation and improved productivity. Regardless of operator skills or the final application, the <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/1489"><strong>Qtegra ISDS Software</strong></a> offers logical, streamlined interface allowing straight forward measurement set-up through analytical Workflows. The software includes auto-stop, standby modes, and other features to minimize intervention. It also allows for integrated data evaluation strategies, customized reports and method development. All of the auto-diagnostics ensure important aspects of the instrument are monitored, maximizing uptime.</p><p><strong>Thermo Scientific™ smartEA option:</strong> This option allows you to focus on your research by combining ease-of-use and unattended analysis to deliver high-precision results. The smartEA option uses the analyzer’s <strong>Thermal Conductivity Detector </strong>(TCD) trace to define the required sample dilutions in the <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/2231"><strong>ConFlo IV Universal Interface</strong></a>. The straightforward automated workflow allows you to analyze very small amounts, such as nitrogen and sulfur, along with highly abundant elements, such as carbon - all from the same sample.</p><h3><strong>Addressing a world of applications</strong></h3><p><strong>For origin and authenticity questions, the EA IsoLink IRMS Platform provides precise and sensitive measurement of the isotope fingerprints - C, N, S, O and H isotopes - a unique chemical signature of samples, helping you gain unique insights into their history and origin.</strong></p><h4><strong>Food authenticity and origin</strong></h4><p><strong>Is the label declaration on my food correct?</strong></p><p>From fruits and vegetables, to wine, honey and coffee, the EA IsoLink IRMS Platform provides isotopic fingerprints ideally suited to determining food integrity.</p><ul><li>Food adulteration</li><li>Food and beverage origin</li><li>Agronomy</li></ul><h4><strong>Environmental</strong></h4><p><strong>What is the source of pollution in the soil, water or air?</strong></p><p>An assessment of individual organic pollutants particles in air contamination (e.g. PM2.5) will be traced with C, N, and S isotope fingerprints.</p><ul><li>Marine science</li><li>Ecology and biology</li><li>Petroleum and exploration</li></ul><h4><strong>Geosciences</strong></h4><p><strong>What was the weather like thousands of years ago?</strong></p><p>By analyzing materials such as sediments, ice cores and speleothems, researchers can understand epochal changes in vegetation, rainfall patterns and temperature.</p><ul><li>Soil science</li><li>Palaeoclimatology research</li></ul><h4><strong>Forensics</strong></h4><p><strong>How can we investigate provenance and dietary preferences?</strong></p><p>From tracing explosives, illegal drugs, counterfeit currency, animal tissues such as ivory, dietary preferences and crime scene evidence, forensic investigations based on isotope fingerprints examine samples’ origin.</p><ul><li>Archaeology</li><li>Provenance</li></ul><h3><strong>Connectivity for origin and authenticity</strong></h3><p>Your lab can focus on isotopic investigations by taking advantage of having one partner and one platform for your elemental and isotope analysis. Thanks to the connectivity of the<strong> </strong><a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/2232"><strong>DELTA Q IRMS</strong></a> and the connecting peripherals that are fully controlled by the <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/1489"><strong>Qtegra ISDS Software</strong></a>, you can also leverage the high throughput, unattended operation and flexibility for demanding analysis, regardless of the applications.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_EA_Iso_Link_IRMS_System_2_dcb8a3d338.jpg" alt="Thermo Scientific™ EA IsoLink™ IRMS System " srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_EA_Iso_Link_IRMS_System_2_dcb8a3d338.jpg 245w," sizes="100vw" width="1464" height="933"></p>

LABTECH Analyser of organically bound halogens and sulphur LTX Unique

The latest model in the line of AOX/EOX analysers is the LTX Unique, which is the successor of the successful LTX-2000+ model

<p><strong>In the last decade, the group parameters of organically bound halogens (AOX, EOX, POX) have become the most monitored indicators in the analysis of environmental samples. What speaks in favour of these group indicators is the constantly increasing number of individual halogenated compounds that need to be monitored in the environment, and the relative speed, simplicity and excellent reproducibility of the entire analytical determination.</strong></p><p>LABTECH has been developing and manufacturing organically bound halogens analysers for over 20 years. The latest model in the line of AOX/EOX analysers is the LTX Unique, which is the successor of the successful LTX-2000+ model.</p><h3><strong>LTX Unique – AOX, EOX, POX and TX analyzer</strong></h3><p>LTX Unique brings easy-to-use, fast and precise determination of halogens to your lab. The modular system is capable to analyze wide range of halogen concentrations in various matrices at high flexibility and low cost operation. It meets with applicable ISO, DIN, EPA and ASTM standards.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/LABTECH_LTX_Unique_AOX_EOX_POX_and_TX_analyzer_6f92cc9a9f.jpg" alt="LABTECH: LTX Unique – AOX, EOX, POX and TX analyzer" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_LABTECH_LTX_Unique_AOX_EOX_POX_and_TX_analyzer_6f92cc9a9f.jpg 245w," sizes="100vw" width="800" height="232"></p><h4><strong>Analysis of Adsorbable Organic Halogens (AOX)</strong></h4><p>Most organic halogens are originated during utilization of different kind of solid and liquide materials and compounds which contain chlorine substances. Monitoring of processes like water treatment, bleaching, refinery and many others industrial processes is important to avoid contamination of environment by organic halogens.</p><p><strong>LTX UNIQUE</strong> is designed to measure organic bound halogens in solid and liquid samples. These halogens are determinated as specific groups of parameters:</p><ul><li><strong>AOX</strong> (Adsorbable Organic Halogens)</li><li><strong>EOX</strong> (Extractable Organic Halogens)</li><li><strong>POX </strong>(Purgeable Organic Halogens)</li><li><strong>TX</strong> (Total Organic Halogens)</li></ul><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/LABTECH_LTX_UNIQUE_Analysis_of_Adsorbable_Organic_Halogens_AOX_e86691384a.jpg" alt="LABTECH: LTX UNIQUE - Analysis of Adsorbable Organic Halogens (AOX)" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_LABTECH_LTX_UNIQUE_Analysis_of_Adsorbable_Organic_Halogens_AOX_e86691384a.jpg 234w," sizes="100vw" width="628" height="419"></p><h4><strong>LTX UNIQUE meets your lab needs</strong></h4><p>This microcoulometric combustion analyzer directly determinates concentrations of usually 10 micrograms per litre in water of organically bound chlorine, bromine and iodine (expressed as chloride or halogens) adsorbable on activated carbon. Higher concentrations are possible by diluting prior to analysis. The AOX analyzer can be used for either <strong>routine determination of halogens</strong> or <strong>R&amp;D</strong> in a wide range of <strong>environmental</strong> and <strong>industrial applications</strong>.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/LABTECH_LTX_UNIQUE_titration_curve_4d327bf3a6.jpg" alt="LABTECH: LTX UNIQUE - titration curve" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_LABTECH_LTX_UNIQUE_titration_curve_4d327bf3a6.jpg 245w," sizes="100vw" width="800" height="269"></p><h4><strong>LTX Unique – highlights of the technology</strong></h4><h5><strong>Furnace</strong></h5><ul><li>High temperature furnace with adjustable temperature control</li><li>Robust combustion tube allows efficient and time-optimized combustion proces</li><li>Pre-treatment before the combustion process</li><li>Same combustion unit for AOX and EOX determination</li></ul><h5><strong>Microcoulometric Titration</strong></h5><ul><li>Durable and easy-to-use titration cell designed by Labtech</li><li>Wide dynamic range and high stability microcoulometer</li><li>Robust and compact electrodes with low and easy maintenance</li><li>Suitable for a separate determination of halides</li></ul><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/LABTECH_LTX_UNIQUE_Microcoulometric_Titration_bc21e40ef0.jpg" alt="LABTECH: LTX UNIQUE - Microcoulometric Titration" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_LABTECH_LTX_UNIQUE_Microcoulometric_Titration_bc21e40ef0.jpg 235w," sizes="100vw" width="700" height="464"></p><h5><strong>Sample Introduction and Measurement</strong></h5><ul><li>Measurement of organic halogens in liquide and solid samples</li><li>Both quarts boats and frits are supported</li><li>Fast and easy switch over between AOX and EOX modules conected to the same measurement unit</li><li>Intuitive application SW quides the operator and save time for analysis</li></ul><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/LABTECH_LTX_UNIQUE_Sample_Introduction_and_Measurement_eec4f7f68e.jpg" alt="LABTECH: LTX UNIQUE - Sample Introduction and Measurement" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_LABTECH_LTX_UNIQUE_Sample_Introduction_and_Measurement_eec4f7f68e.jpg 235w," sizes="100vw" width="700" height="464"></p><h4><strong>Determination of Organic Halogens</strong></h4><p>LTX Unique meets with all requirement in AOX analysis and other international and local standards are also supported (e.g. EOX, POX and TX methods). Halogens can be determined from a wide range of matrices by combustion process and microcoulemetric measurement. The following examples can give an overview how organically bound halogens are determinated:</p><ul><li><h5><strong>AOX (Adsorbable Organic Halogens)</strong></h5><ul><li>according to ISO 9562, DIN EN 9562, DIN 38 414-S18, ASTM D 4744-89, EPA Method 450.1, EPA Test Method 9020</li><li>Halogens are measured by sorption of organohalides from the aqueous sample on activated charcoal according to standardizes procedures. This charcoal is introduced to cumbustion tube.</li></ul></li><li><h5><strong>EOX (Extractable Organic Halogens)</strong></h5><ul><li>according to NEN 6402, DIN 38409-H8, DIN 38414-S17.</li><li>These organic halogens are determinated by extraction with low polar solvent.</li></ul></li><li><h5><strong>POX (Purgeable Organic Halogens)</strong></h5><ul><li>according DIN 38414-S17, EPA Test Method 9021</li><li>Volatile organic halogens as purched components are measured from water or suspension in inert gas at certain temperature.</li></ul></li><li><h5><strong>TX (Total Organic Halogens)</strong></h5><ul><li>according to EPA 9076</li><li>Determination of TX is run on a wide range of liquid hydrocarbon samples without any separation.</li></ul></li></ul><h4><strong>Specifications of LTX UNIQUE</strong></h4><ul><li><strong>Dimensions:</strong> 970 x 360 x 295 mm (W x D x H)</li><li><strong>Weight: </strong>27 kg</li><li><strong>Furnace temp</strong>.: Max. 1100 °C</li><li><strong>Power supply:</strong> 230 V / 50 Hz, max.1100 W</li><li><strong>Gas requirements: </strong>Oxygen 99.6 % (AOX/EOX)</li><li><strong>Argon: </strong>99.996 % (EOX)</li><li><strong>Software: </strong>ENGINE LT</li><li><strong>PC: </strong>Windows® 10</li><li><strong>Detector: </strong>Microcoulometer with Ag indication electrode</li><li><strong>Titration currents:</strong> 2000, 200, 20 and 2 uA</li><li><strong>Measuring range:</strong> 0,1 - 300 µg Cl-</li><li><strong>Limit of detection: </strong>0,02 µg Cl-</li></ul>

LECO TruSpec Micro CHN/CHNS/O

TruSpec Micro provides fast, reliable CHN, CHNS, and optional oxygen analysis of micro samples with low cost-per-analysis, robust design, and rapid results in as little as 4 minutes.

<p><strong>The TruSpec Micro delivers high-performance determination of carbon, hydrogen, nitrogen, sulfur, and oxygen in solid or liquid micro samples. Its integrated design combines speed, robustness, and low maintenance to provide reliable and consistent elemental analysis, even for demanding laboratory workflows.</strong></p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/LECO_Tru_Spec_Micro_CHN_CHNS_O_4090ff8fc5.jpg" alt="LECO: TruSpec Micro CHN/CHNS/O" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_LECO_Tru_Spec_Micro_CHN_CHNS_O_4090ff8fc5.jpg 218w," sizes="100vw" width="1202" height="862"></p><h4><strong>Key Features</strong></h4><ul><li>Optimal performance for CHN, CHNS, and optional oxygen determination in micro samples</li><li><strong>Low cost-per-analysis</strong> with minimal reagent consumption</li><li><strong>Nominal sample mass of 2 mg</strong>, ideal for limited or valuable samples</li><li><strong>Rapid analysis times</strong> (approximately 4 minutes for CHN/CHNS)</li><li>Reduced downtime and maintenance due to robust system design</li><li>Supports compliance with <strong>21 CFR Part 11</strong> regulations</li><li>Optional <strong>oxygen module</strong> enables independent oxygen determination using high-temperature pyrolysis at <strong>1300 °C</strong>, with analysis times of about 2 minutes</li></ul><h4><strong>Theory of Operation</strong></h4><p>The TruSpec Micro CHN and CHNS systems achieve their efficiency and speed through a flow-through carrier gas design combined with highly selective infrared (IR) and thermal conductivity (TC) detectors.</p><p>A weighed micro sample is placed into the autoloader and automatically introduced into a high-temperature combustion furnace. During combustion, carbon is converted to CO₂, hydrogen to H₂O, nitrogen to N₂, and sulfur to SO₂. The resulting gases are swept from the furnace through scrubbing reagents and directed to the detection system as they are released. Independent IR detectors simultaneously measure carbon, hydrogen, and sulfur, while nitrogen is quantified using a thermal conductivity detector. The complete CHN or CHNS analysis cycle is finished in approximately four minutes.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/LECO_Tru_Spec_Micro_CHN_CHNS_O_2_be47a94ba1.jpg" alt="LECO: TruSpec Micro CHN/CHNS/O" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_LECO_Tru_Spec_Micro_CHN_CHNS_O_2_be47a94ba1.jpg 204w," sizes="100vw" width="855" height="654"></p><h4><strong>Optional Oxygen Determination</strong></h4><p>The micro oxygen add-on module extends the TruSpec Micro’s capabilities to oxygen analysis in organic matrices and is compatible with both CHN and CHNS configurations. Samples are introduced into a dedicated high-temperature pyrolysis furnace, where oxygen reacts in a carbon-rich environment to form CO. The CO is then converted to CO₂ and measured by an infrared detector. Oxygen analysis is completed in roughly one to two minutes, depending on configuration.</p><h4><strong>Models</strong></h4><ul><li><strong>TruSpec Micro CHNS</strong> – Carbon, Hydrogen, Nitrogen, and Sulfur determination</li><li><strong>TruSpec Micro CHN</strong> – Carbon, Hydrogen, and Nitrogen determination</li></ul><h4><strong>Options</strong></h4><ul><li>Sulfur add-on module</li><li>Oxygen add-on module</li></ul>

LECO RC612 Multiphase Determination of Carbon and Water

The LECO RC612 delivers fast carbon and water determination with advanced carbon form differentiation, flexible furnace programming, IR detection, and optional automation in a compact, easy-to-use system.

<p><strong>The RC612 is a state-of-the-art analyzer designed for fast and reliable determination of carbon and water in a wide range of organic and inorganic materials. In addition to total carbon and moisture quantification, the RC612 enables differentiation between multiple carbon forms, providing deeper insight into sample composition. Its compact footprint, robust construction, and intuitive operating software make it a powerful yet easy-to-use solution for routine and advanced laboratory applications.</strong></p><h4><strong>Key Features</strong></h4><ul><li>Complies with <strong>AWS (ANSI) approved methods</strong> for determination of moisture content in welding fluxes and welding electrode flux coverings</li><li>Supports both <strong>qualitative and quantitative analysis</strong></li><li><strong>Easy-to-install combustion tube</strong> simplifies maintenance and reduces downtime</li><li>Large-diameter reaction tube enables moisture analysis of diverse sample types, including powders, flat strips, and tubular sections</li><li>Differentiation of <strong>surface, free, organic, and inorganic carbon</strong> forms</li><li>Optional <strong>rugged 50-position autoloader</strong> for unattended, automated operation</li><li>Built-in <strong>on-board diagnostics</strong> to minimize downtime and support reliable performance</li></ul><h4><strong>Theory of Operation</strong></h4><p>The RC612 multiphase carbon and hydrogen/moisture determinator measures carbon and water content in organic and inorganic samples while distinguishing between different carbon sources. The system employs a dual-stage furnace with advanced temperature control, programmable from near ambient up to 1100 °C, allowing tailored thermal programs for specific applications.</p><p>During analysis, the operator can define multiple furnace steps and select either oxygen or nitrogen as the purge gas to create oxidizing or inert conditions. Under these controlled environments, carbon- and water-containing components are either combusted or reacted. An integrated afterburner furnace, typically operated at 850 °C, together with a secondary oxidation catalyst, ensures complete conversion of all evolved components.</p><p>Quantification is performed using <strong>infrared (IR) detection</strong>, with results reported as weight percent or coating weight (mg/in²). When samples are combusted in an oxidizing atmosphere, nearly all carbon forms are converted to CO₂. Organic carbon is identified by the simultaneous formation of CO₂ and H₂O, producing coincident IR signals. In inert conditions, water and carbonates are detected while organic carbon is generally not observed, enabling selective differentiation of carbon species.</p><p>For unknown samples, a slow temperature ramp program (for example, 100 °C to 1000 °C at 20 °C/min) can be applied. This approach reveals the temperatures at which various carbon forms oxidize or volatilize, allowing optimization of furnace programs for faster and more targeted quantitative analysis in routine workflows.</p>

LECO DH603 Residual and Diffusible Hydrogen Determination by Hot Extraction

The LECO DH603 delivers fast, precise residual and diffusible hydrogen determination in ferrous alloys using hot extraction, advanced furnace control, and flexible sampling options.

<p><strong>The DH603 Hot Extraction Analyzer is designed for fast, precise determination of hydrogen in iron and ferrous alloys. It supports residual (total) hydrogen analysis as well as combined diffusible and residual hydrogen determination using a single, compact instrument. With a small footprint, intuitive operating software, enhanced safety features, and a robust mechanical design, the DH603 streamlines hydrogen analysis in both production and quality control environments.</strong></p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/LECO_DH_603_Stanoveni_zbytkoveho_a_difuzniho_vodiku_horkou_extrakci_d968c7c42b.jpg" alt="LECO: DH603 Residual and Diffusible Hydrogen Determination by Hot Extraction" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_LECO_DH_603_Stanoveni_zbytkoveho_a_difuzniho_vodiku_horkou_extrakci_d968c7c42b.jpg 237w," sizes="100vw" width="1325" height="875"></p><h4><strong>Key Features</strong></h4><ul><li>Exclusive <strong>ECLIPSE architecture</strong>, a LECO-designed platform that improves long-term reliability and simplifies serviceability</li><li>Support for a wide range of <strong>evacuated pin tubes and diffusible samplers</strong> for rapid hydrogen determination in molten metals</li><li>Improved internal plumbing for faster and easier maintenance of the gas flow path</li><li>Ergonomic outer shells provide <strong>easy access to critical components</strong> for routine operation and service</li><li>Advanced furnace control system enabling <strong>temperature ramping from ambient to 1100 °C</strong></li><li>Optional <strong>diffusible sampler piercer</strong>, allowing users to choose between residual/total hydrogen or combined diffusible and residual hydrogen measurements</li><li><strong>Gas dose calibration</strong> capability enables calibration without the need for reference materials</li></ul><h4><strong>Theory of Operation</strong></h4><p>The DH603 determines hydrogen content in iron and ferrous alloys using hot extraction coupled with thermal conductivity detection. The system supports two analytical approaches: residual (total) hydrogen determination and combined diffusible plus residual hydrogen determination when equipped with the optional piercer.</p><p>For <strong>residual (total) hydrogen analysis</strong>, a pre-weighed sample is placed directly into the furnace. Hydrogen is released from the sample by hot extraction and carried into a flowing inert gas stream. The evolved hydrogen is quantified using a thermal conductivity detector, and results are reported in parts per million (ppm). Samples are typically collected using LECO vacuum pin tubes or equivalent techniques.</p><p>For <strong>diffusible and residual hydrogen analysis</strong>, a sampler is first placed into the optional piercing unit. The sampler is punctured, allowing diffusible molecular hydrogen to be purged into the carrier gas stream and measured by the thermal conductivity detector. After diffusible hydrogen measurement, the sampler is removed, the outer shroud is taken off, and the remaining pin sample is weighed. This sample is then introduced into the furnace, where residual hydrogen is released by hot extraction and quantified. Final hydrogen concentrations are reported in ppm, providing a complete hydrogen profile from a single instrument.</p><h4><strong>Available Models</strong></h4><ul><li><strong>DH603DC</strong> – DH603 with diffusible hydrogen piercer</li><li><strong>DH603C</strong> – DH603 for residual (total) hydrogen determination</li></ul>

Products from category Elemental Analyzers - page 2

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