<p><strong>Our Library never stops expanding. What are the most recent contributions to LabRulezGCMS Library in the week of 31st August 2026? Check out new documents from the field of the gas phase, especially GC and GC/MS techniques!</strong></p><blockquote><p><span style="font-size:20px;">👉 </span><a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/library"><span style="font-size:20px;"><strong>SEARCH THE LARGEST REPOSITORY OF DOCUMENTS ABOUT GCMS AND RELATED TECHNIQUES</strong></span></a></p></blockquote><blockquote><p><strong>👉 Need info about different analytical techniques?</strong> Peek into <a target="_blank" rel="noopener noreferrer" href="https://lcms.labrulez.com/library"><strong>LabRulezLCMS</strong></a> or <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library"><strong>LabRulezICPMS</strong></a> libraries.</p></blockquote><p>This week we bring you application notes by <strong>Agilent Technologies</strong>, <strong>Shimadzu, Thermo Fisher Scientific </strong>and presentation by<strong> MDCW / Liège University!</strong></p><h3><strong>1. Agilent Technologies: Extend the time window for the detection of low level anabolic‑androgenic steroids and their metabolites</strong></h3><p><strong>Steroid profiling, screening, and confirmatory analysis using the </strong><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/gcms/library?mainauthorItems=10&amp;search=7010"><strong>Agilent&nbsp;7010 GC/MS mass spectrometer</strong></a></p><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/pdf/5991_9045_EN_Doping_Control_App_Note_1_13dde5f053.pdf"><strong>Full PDF for download</strong></a></li></ul><section><div><div><div><div><div><div><p>Doping laboratories want to have lower detection limits to be able to identify and quantitate illegal drugs for a longer time window between doping and urine sample collection. This Application Note describes how the doping control lab in Kreischa, Germany used the Agilent 7010 Triple Quadrupole GC/MS System (TQ) for enhanced targeted detection of anabolic‑androgenic steroids in urine samples. The 7010 TQ enabled higher sensitivity, longer maintenance-free intervals, and more stable operation than earlier models, and satisfied all measurement specifications required by the World Anti‑Doping Agency (WADA). The 7010 TQ GC/MS ion source produces more ions, and provides exceptional sensitivity for the detection of low intensity metabolites weeks after drug ingestion. However, this higher sensitivity may lead to saturation of endogenous components naturally present at higher concentrations. This method provides a sensitive and robust operation over a wide concentration range, permitting the detection of low-concentration exogenous species in the presence of high‑concentration endogenous species, which can vary with ethnicity.</p><h4><strong>Experimental</strong></h4><p>The <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/gcms/library?mainauthorItems=10&amp;search=7010"><strong>Agilent 7010 GC/TQ system</strong></a> consists of an <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/gcms/library?mainauthorItems=10&amp;search=7890"><strong>Agilent 7890 GC</strong></a> with multimode inlet and backflush, an<strong> Agilent 7993A</strong>, and the Agilent 7010 TQ mass spectrometer.</p><h4><strong>Conclusions&nbsp;</strong></h4><p>Based on the method optimization and thorough testing at the Kreischa lab, an Agilent 7010 GC/MS-based protocol was developed. This protocol fulfills the screening and confirmation requirements of steroid measurements in doping control labs. With this method, it is possible to detect traces of exogenous anabolic steroid metabolites while quantifying small concentrations of testosterone and epitestosterone typical in Asian populations. It permits the measurement of high‑abundance endogenous steroids such as androsterone and etiocholanolone in the same injection, while analyzing testosterone/epitestosterone and androsterone/etiocholanolone ratios without suppression.&nbsp;</p><p>The backflush capability of the system protects the analytical column, and consequently the mass spectrometer, by removing heavy matrix components. This allowed more than 6,000 samples to be analyzed on the same column without requiring ion source cleaning or filament change. It also demonstrated that the higher, 130&nbsp;eV electron energy did not sacrifice the filament lifetime. It performed reliable measurements of both trace (0.2&nbsp;pg on‑column) and high (10,000&nbsp;pg on‑column) concentration analytes in the same run.&nbsp;</p><p>The method validation revealed that the exceptional sensitivity offered by the 7010 GC/MS can be used to:&nbsp;</p><ul><li>Improve the trace detection ability of the method&nbsp;</li><li>Reduce the amount of sample&nbsp;injected&nbsp;</li><li>Extend maintenance-free intervals</li></ul><h3><strong>2. MDCW / Liège University: The Century Mix: updates and cool projects</strong></h3><ul><li>Presentation</li><li><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/pdf/DG_1_Dimandja_Stefanuto_34c4a66c3d.pdf"><strong>Full PDF for download</strong></a></li></ul><section><div><div><div><div><div><div><p>The presentation <strong>“The Century Mix: updates and cool projects”</strong> introduces the Century Mix, a standardized reference mixture developed for comprehensive two-dimensional gas chromatography (GC×GC). The mixture contains <strong>100 compounds representing a broad range of chemical classes</strong>, including alkanes, alcohols, ketones, esters, lactones, phthalates, and aromatic compounds. Stability was a key criterion in compound selection, and the mixture was developed through cross-laboratory collaboration for <strong>column characterization, method assessment, and quality control</strong>. Its structured chromatographic behavior also makes it useful for studying how different compound classes behave in GC×GC separations.</p><p>A major part of the work examined the <strong>factors influencing retention indices (RI) in GC×GC systems</strong>, which are important for reliable compound annotation in non-targeted analysis. An inter-laboratory study involved <strong>11 GC×GC systems</strong> using cryogenic, Peltier, and flow modulation, different detectors, and both normal and reversed column configurations. Principal component analysis showed clear grouping according to normal versus reversed orthogonality, confirming the strong influence of stationary-phase configuration. A subsequent design-of-experiments study evaluated <strong>140 combinations</strong> of temperature ramp rate, carrier-gas flow rate, modulation period, and secondary-oven temperature offset.</p><p>The results showed that the influence of experimental conditions is strongly <strong>compound dependent</strong>. Of the compounds evaluated in the statistical model, 33 showed RI variation that could be linked to the investigated parameters, whereas 43 did not follow the model well. Compounds such as quinoline, phthalates, lactones, terpenes, and some aromatic compounds showed particularly pronounced effects. For quinoline, for example, the model explained about <strong>93% of RI variability</strong>, with differences of approximately 75 RI units across the tested conditions, while 2-hexanone showed considerably weaker dependence. Overall, <strong>temperature ramp rate and flow rate emerged as particularly important parameters</strong>, although the magnitude of their effect depended on compound chemistry and column configuration.</p><p>The Century Mix is therefore being developed not only as a characterization mixture but also as a tool for <strong>system quality control and more reliable retention-index prediction</strong>. Repeated standardized QC measurements demonstrated very low RI variability and can be used to monitor system stability, experimental effects, and potential instrument drift. The broader goal is to better understand the fundamental chemistry governing GC×GC retention and ultimately improve method development, data processing, and identification of unknown compounds by combining high-quality separations, mass spectra, and predicted retention information.</p><h3><strong>3. Shimadzu: Determination of Free and Total Glycerol and Mono-, Di-, and Triglyceride Contents in Biodiesel According to EN 14105</strong></h3><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/pdf/an_05_sca_180_055_en_9b8677ed6a.pdf"><strong>Full PDF for download</strong></a></li></ul><h4><strong>User benefits</strong></h4><ul><li><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/gcms/library?mainauthorItems=1&amp;search=2060"><strong>Nexis GC-2060</strong></a> offers reliable analysis of biodiesel samples regarding their free and total glycerol and mono-, di-, and triglyceride contents, using hydrogen as a cost-effective carrier gas&nbsp;</li><li>Hydrogen carrier gas can be used safely through built-in safety measures</li><li>The multi-mode injection unit (MMI) allows selection of the preferred injection mode – direct (simple OCI) or convenient splitless PTV mode – both delivering excellent instrument performance in line with the standard’s requirements</li></ul><p>Playing a vital part in countries’ efforts to lower greenhouse gas emissions, biofuels can be manufactured from various feedstocks such as vegetable oils, animal-derived fats, and recycled cooking oils. Biodiesel production predominantly uses rapeseed, soybean, and palm oils. Because feedstocks are so varied, ongoing quality monitoring is essential - since the raw material’s quality greatly influencesthe final biodiesel quality.&nbsp;</p><p>The EN 14105:2024 describes the determination of free and total glycerol contents and mono-, di-, and triglyceride contents in biodiesel by means of gas chromatography with flame ionization detection (GC-FID). Injection shall be performed via on-column injector or an equivalent device<sup>1</sup>.&nbsp;</p><p>This study shows the analysis of biodiesel originating from rapeseed, soybean, and palm oil using the Nexis GC-2060 gas chromatograph and its multi-mode injection unit (MMI).</p><h4><strong>Configuration and Analysis Conditions</strong></h4><p>Gas chromatograph <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/gcms/library?mainauthorItems=1&amp;search=2060"><strong>Nexis GC-2060</strong></a> with multi-mode injection unit (MMI), flame-ionization detector (FID) and autosampler <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/gcms/library?mainauthorItems=1&amp;search=AOC+-30i"><strong>AOC -30i</strong></a>.</p><h4><strong>Conclusion&nbsp;</strong></h4><p>Nexis and AOC are trademarks of Shimadzu Corporation or its affiliated companies in Japan and/or other countries.. Nexis GC-2060 provides reliable analysis of biodiesel samples for glycerol and glyceride contents according to EN 14105:2024 across the commonly used feedstocks. It supports hydrogen as a cost-effective carrier gas, while the multi-mode injection unit (MMI) offers selection of the injection mode based on user preference: direct mode representing simple on-column (OCI) analysis or splitless programmed temperature vaporization (PTV) mode as a convenient alternative that delivers comparable performance.</p><h3><strong>4. Thermo Fisher Scientific: Streamlined static headspace GC–MS approach for detection of impurities in recycled PET</strong></h3><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/pdf/an_004458_gc_ms_impurities_recycled_pet_an004458_na_en_6cb2435671.pdf"><strong>Full PDF for download</strong></a></li></ul><p>Polyethylene terephthalate (PET) is a widely used thermoplastic polymer valued for its strength, low weight, durability, and adaptability. Owing to these properties, it is extensively applied in packaging, textile fibers, and electronic components. PET is particularly suitable for recycling because it can be melted and reshaped multiple times with minimal loss of performance, and it is easily recognizable by the recycling code “1” (♳). The recycling of PET involves several stages, including collection, sorting, transport, processing, washing, pelletizing, and remanufacturing into new products [1]. However, during these steps, contaminants such as plasticizers, residual monomers, and degradation byproducts may be introduced.&nbsp;</p><p>The presence of such substances can pose potential risks to both environmental and human health, making the identification and characterization of contaminants in recycled PET essential for evaluating material quality and safety. Among the non-intentionally added substances (NIAS), benzene, acetaldehyde, and limonene are of particular relevance. Benzene is a recognized carcinogen and represents a serious health concern if present in PET. It may form as a degradation product of PET, with the reaction catalyzed by acidic compounds released at high temperatures by polymer impurities such as polyvinyl chloride (PVC). Poor temperature control or overheating can increase benzene formation as a degradation byproduct. Acetaldehyde, another degradation product of PET generated during bottle manufacturing, can alter the sensory properties of bottled beverages. Limonene, a flavor compound commonly present in soft drinks, may be absorbed into recycled PET and subsequently migrate into packaged beverages, potentially affecting product quality.&nbsp;</p><p>Gas chromatography coupled to headspace sampling is a fast and simple technique that enables the extraction of volatile and semivolatile compounds from solid and liquid samples without the need for time-consuming sample preparation.&nbsp;</p><p>In this study, headspace sampling coupled to single quadrupole mass spectrometry was used to assess the overall quantitative performance for analysis of acetaldehyde, benzene, and limonene in recycled PET packaging.&nbsp;</p><p>The capability of the Thermo Scientific™ ISQ™ 7610 single quadrupole GC–MS of combining the simultaneous acquisition of both single ion monitoring (SIM) and full scan (FS) allowed for sensitive targeted analysis as well as screening of unknown contaminants possibly present in recycled PET bottles.</p><h4><strong>Experimental&nbsp;</strong></h4><p>In all experiments, a <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/64"><strong>TriPlus 500 HS autosampler</strong></a> was coupled to a <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/486"><strong>Thermo Scientific™ TRACE™ 1610 Gas Chromatograph (GC)</strong></a>, configured with a Thermo Scientific™ iConnect™ Split/splitless Injector Module (iConnect-SSL), and connected to an <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/484"><strong>ISQ 7610 single quadrupole mass spectrometer</strong></a>.&nbsp;</p><p>The separation of the target analytes was achieved using a <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/1751"><strong>Thermo Scientific™ Trace GOLD™ TG-624 SILMS capillary column</strong></a>, 60 m x 0.25 mm x 1.4 µm (Part No. 26059-3330). This column provides a low to mid polarity phase with high thermal stability (maximum operating temperatures up to 320 °C) and high inertness, enabling Gaussian peak shapes for analysis of volatile organics. The TriPlus 500 HS autosampler is connected directly to the analytical column, removing the use of a long external transfer line. In this configuration, the SSL injector module is used only for the pneumatic control of the carrier gas and split flow.</p><h4><strong>Conclusions&nbsp;</strong></h4><p>The results presented in this work demonstrate that headspace coupled to GC–MS provides a suitable and simple solution for analysis of contaminants in rPET, with no complex sample preparation required.&nbsp;</p><ul><li>The capability of combining FS with SIM acquisition allows for qualitative and quantitative analysis, increasing confidence in compound identification through spectral comparison with NIST library and allowing for the detection of possible analyte co-elution.&nbsp;</li><li>The TriPlus 500 HS autosampler provides highly repeatable solventless extraction from solid samples with absolute area counts RSD &lt; 5%, permitting reliable and consistent quantitative data.&nbsp;</li><li>The ISQ 7610 single quadrupole GC–MS demonstrates an extended linear response (≥ 4–5 orders of magnitude) with R2 ≥ 0.997, calculated amounts within ± 20% the expected value, and ion ratio deviation ≤ 15% across the calibration curve.&nbsp;</li><li>Sensitivity was demonstrated with overall calculated LOD ≤ 0.03 ng/µL.</li><li>Chromeleon CDS helps ensure data integrity, traceability, and effective data management from instrument control to the final report streamlining analysis and data review processes.</li></ul></div></div></div></div></div></div></section></div></div></div></div></div></div></section>

News from LabRulezGCMS Library - Week 36, 2026

News from LabRulezLCMS Library - Week 36, 2026

<p><strong>Our Library never stops expanding. What are the most recent contributions to LabRulezICPMS Library in the week of 31st August 2026? Check out new documents from the field of spectroscopy/spectrometry and related techniques!</strong></p><blockquote><p><span style="font-size:20px;">👉 </span><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library"><span style="font-size:20px;"><strong>SEARCH THE LARGEST REPOSITORY OF DOCUMENTS ABOUT SPECTROSCOPY/SPECTROMETRY RELATED TECHNIQUES</strong></span></a></p></blockquote><blockquote><p><strong>👉 Need info about different analytical techniques?</strong> Peek into <a target="_blank" rel="noopener noreferrer" href="https://lcms.labrulez.com/library"><strong>LabRulezLCMS</strong></a> or <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/library"><strong>LabRulezGCMS</strong></a> libraries.</p></blockquote><p>This week we bring you brochures by <strong>Agilent Technologies </strong>and<strong> Waters Corporation </strong>and application notes by <strong>Shimadzu </strong>and<strong> Thermo Fisher Scientific!</strong></p><h3><strong>1. Agilent Technologies: Agilent OpenLab ICP-MS Software</strong></h3><p><strong>Simplify every step of ICP-MS analysis</strong></p><p><strong>For Agilent </strong><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/icpms/library?mainauthorItems=10&amp;search=7800"><strong>7800</strong></a><strong>, </strong><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/icpms/library?mainauthorItems=10&amp;search=7850"><strong>7850</strong></a><strong>, and </strong><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/icpms/library?mainauthorItems=10&amp;search=7900"><strong>7900</strong></a><strong> ICP-MS systems, and Agilent </strong><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/icpms/library?mainauthorItems=10&amp;search=8900"><strong>8900</strong></a><strong> and </strong><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/icpms/library?mainauthorItems=10&amp;search=9500"><strong>9500 ICP-QQQ</strong></a><strong> systems.</strong></p><ul><li>Brochure</li><li><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/pdf/br_openlab_icp_ms_software_5994_9288en_agilent_05f01dcdef.pdf"><strong>Full PDF for download</strong></a><strong>&nbsp;</strong></li></ul><p>The brochure introduces <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/icpms/library?mainauthorItems=10&amp;search=OpenLab+ICP-MS+Software"><strong>Agilent OpenLab ICP-MS Software</strong></a>, designed to simplify routine operation and data handling for <strong>Agilent 7800, 7850, and 7900 ICP-MS systems</strong> and the <strong>8900</strong> and <strong>9500</strong> <strong>ICP-QQQ systems</strong>. The software supports the complete analytical workflow—from checking instrument readiness and creating batches to acquisition, data review, reporting, and compliance. A central dashboard provides an overview of system status, maintenance requirements, instrument health, and utilization, while Smart EMF and post-run performance checks help users identify when maintenance may be required. Guided Diagnostics, Meter Monitor, and time-stamped system records also support troubleshooting by tracking parameters such as vacuum levels, gas flows, and temperatures.</p><p>Method and batch setup are designed to reduce manual configuration. Batches can be created from preset methods, templates, existing batches, Method Wizard, or Method Advisor, and legacy Agilent ICP-MS MassHunter batches can be opened directly in OpenLab ICP-MS. For the <strong>9500 ICP-QQQ</strong>, Method Advisor provides an element-focused approach in which users select target elements and calibration information while the software applies recommended acquisition masses and cell-gas conditions. Preset methods are available for applications including <strong>EPA 200.8/EPA 6020, USP &lt;232&gt;, ICH Q3D, and Chinese Pharmacopoeia requirements</strong>, while an IntelliQuant Screening preset supports semiquantitative screening of unknown samples. Routine instrument tasks can also be automated through autotuning, startup checks, batch queues, end-of-run verification, rinse functions, and automatic shutdown.</p><p>For data evaluation, OpenLab ICP-MS provides a real-time workspace where users can review analyte concentrations, internal-standard recoveries, stability plots, spectra or chromatograms, calibration information, QC charts, and IntelliQuant results in a single view. <strong>IntelliQuant</strong> acquires a complete mass spectrum and displays semiquantitative elemental concentrations using a color-coded periodic table, while <strong>IntelliQuant Star Rating</strong> assigns a zero-to-five-star data-quality score based on factors such as potential interferences, calibration quality, background, detection limits, and precision. Reporting options include whole-batch reports, elemental impurity reports for USP &lt;232&gt;/&lt;233&gt; and ICH Q3D, customizable reports, structured CSV export, and direct data transfer to LIMS.</p><p>The software can be expanded for specialized applications, including <strong>LC-ICP-MS and GC-ICP-MS</strong>, advanced QC workflows, single-particle ICP-MS and FFF-ICP-MS, ADS 2 automation, semiconductor analysis, and peripheral-device control. Supported analytical approaches include external calibration, standard additions, semiquantitative calibration, isotope ratios, and isotope dilution. For regulated laboratories, OpenLab ICP-MS can be combined with scalable OpenLab compliance solutions providing electronic signatures, user access control, configurable roles, system activity logs, and audit trails, supporting workflows subject to <strong>21 CFR Part 11, EU Annex 11, and equivalent regulations</strong>. Overall, the platform is positioned as a unified environment for routine and advanced ICP-MS workflows, combining instrument control, method setup, diagnostics, data-quality assessment, reporting, and compliance support.</p><h3><strong>2. Shimadzu: Identification of Virgin PET and Recycled PET by X-ray Fluorescence Spectrometry</strong></h3><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/pdf/an_01_01204_en_f3f20ff020.pdf"><strong>Full PDF for download</strong></a></li></ul><h5><strong>User benefits</strong></h5><ul><li>EDX enables the identification of recycled PET.&nbsp;</li><li>Measurements are quick and simple, require no cumbersome pretreatment, and can be automated using a multi-sample turret.&nbsp;</li><li>The instrument offers excellent cost-performance and supports the detection of a wide range of elements.</li></ul><p>Establishing a sustainable circular economy is a major societal challenge, and recycling plastic materials such as PET (polyethylene terephthalate) plays a particularly important role in reducing environmental impact. Large numbers of PET bottles and molded products are used every day in the food and beverage sectors. To recycle these materials safely and reliably, technologies are required that can accurately identify their origin. In practice, however, appearance and conventional physical properties alone are insufficient to distinguish virgin material from recycled material, creating a need for a more reliable identification method.&nbsp;</p><p>For rapid identification in industrial settings, a method requiring little or no pretreatment is highly desirable. In some cases, nondestructive analysis is also needed to enable subsequent application of other analytical techniques. This article presents a practical approach in which metal catalysts present in PET are detected by EDX (Energy-Dispersive X-ray Spectroscopy) and used to distinguish material-recycled PET from virgin PET.</p><h4><strong>Principle and Overview&nbsp;</strong></h4><p>Metal catalysts such as antimony (Sb) and germanium (Ge) are used in the synthesis of PET resin. These catalyst metals have been reported to be useful indicators of material origin. 1),2) For example, Sb and Ge are frequently detected together in material-recycled PET, whereas only one catalyst metal is detected in chemically recycled PET and virgin PET. This likely reflects the fact that material-recycled PET is derived from a mixture of feedstocks using different catalysts.&nbsp;</p><p>ICP-AES (ICP optical emission spectrometry) and ICP-MS (ICP mass spectrometry), which are commonly applied to catalyst metal analysis, provide high sensitivity and accuracy. However, they require pretreatment to convert the sample into a solution, thereby lengthening the analytical workflow. By contrast, EDX can measure solid samples directly, making it well-suited to applications requiring rapid results, such as incoming material inspection and in-line analysis in molding plants. Because EDX is non-destructive, it is also suitable for multimodal analytical workflows.&nbsp;</p><p>On the other hand, some commercially available handheld EDX instruments do not support elements such as Sb and Ge. At the same time, higher-end systems may not offer the specifications or price range needed for industrial deployment. The <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/icpms/library?mainauthorItems=1&amp;search=EDX-7200"><strong>EDX-7200</strong></a> supports a broad range of elements with excellent cost performance. This article describes the analysis of Sb and Ge in PET using this instrument.</p><h4><strong>Conclusion&nbsp;</strong></h4><p>EDX enables rapid and straightforward elemental analysis without cumbersome sample pretreatment. Previous studies have shown that the presence of Sb and Ge can be used to identify recycled PET. Building on this concept, this article presents a practical analytical approach based on EDX. Using the EDX-7200, which combines broad elemental coverage with excellent cost performance, the proposed method provides a practical tool for rapid on-site identification, quality control, and traceability management. When combined with physical property data and other information, this approach is expected to contribute to the safety assessment and quality assurance of recycled materials, thereby supporting a more advanced circular economy.</p><h3><strong>3. Thermo Fisher Scientific: Optimizing lithium-ion battery recycling operations using handheld XRF analysis</strong></h3><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/pdf/lithium_ion_battery_recycling_handheld_xrf_analysis_an1120_en_4c00477b78.pdf"><strong>Full PDF for download</strong></a></li></ul><p>The shift to a low-carbon economy and the adoption of electric vehicles will drive an exponential increase in the demand for lithium-ion batteries. As a corollary to this, the International Energy Agency expects the demand for some key commodities to increase significantly over the next two decades: the demand for Copper (Cu) is anticipated to increase by more than 40%; for nickel (Ni) and cobalt (Co), by 60-70% each; and for lithium (Li), by nearly 90%.¹ This will translate into increased mining activities and potentially generate larger amounts of deleterious waste.&nbsp;</p><p>To reduce the environmental impact and limit reliance on scarce commodities associated with economical and geopolitical implications, several countries have implemented regulations regarding producers’ responsibilities.² These regulations contain both incentives and accountability guidelines for lithium-ion battery and electric vehicles manufacturers. Their goal is to facilitate the emergence of a circular economy in which recycling will increasingly contribute to the supply of the strategic raw materials.&nbsp;</p><p>Lithium-ion batteries are made of multiple components, the most valuable being the cathode that contains between 40 and 70% ³, ⁴ of the total value of the battery, depending on its exact chemistry. As of 2023, lithium nickel cobalt manganese oxides (NCM) account for 66% of lithium-ion battery cathode active materials for electric vehicles, followed by lithium iron phosphates (LFP) which account for 24%, and lithium nickel cobalt aluminum oxide (NCA) accounts for the remaining 10%.³</p><h4><strong>Handheld X-ray Fluorescence Analysis&nbsp;</strong></h4><p>Handheld X-ray fluorescence analysis (HHXRF) is an elemental analysis technique that has proven to be cost-effective in recycling areas such as scrap metal and automotive catalytic converters. HHXRF can measure elements from magnesium (Mg) to uranium (U) in various types of materials such as metals and alloys; non-metallic inorganic materials such as ceramics; or ores or plastics. The <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/1993"><strong>Thermo Scientific™ Niton™ XL2</strong></a> and <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/1992"><strong>Thermo Scientific™ Niton™ XL5 Plus Handheld XRF Analyzers </strong></a>deliver accurate elemental analysis in real time, with little or no sample preparation, across multiple steps of the lithium-ion battery recycling workflow. Although handheld XRF does not detect lithium, it can measure most elements from the periodic table including nickel or cobalt which often command much higher value than the lithium in a lithium-ion battery.⁴</p><h4><strong>Conclusion&nbsp;</strong></h4><p>There is no ideal process to recycle lithium-ion batteries that simultaneously incorporates low environmental impact, high metal recovery yield, and economic viability. Because of the variety of technologies and materials used, recycling lithium-ion batteries is a complex journey with multiple possible paths. HHXRF helps recyclers by generating lab-quality data in real time, allowing them to optimize their processes and make fast decisions that generate significant benefits:&nbsp;</p><ul><li>Unwanted materials containing heavy metals such as lead or cadmium can be prevented from entering subsequent steps in the recycling workflow.&nbsp;</li><li>Materials can be accurately sorted and adequate processes for recovery selected depending on the material type (e.g., LFP vs. MCM).&nbsp;</li><li>The economic value of incoming and outgoing material can be more accurately estimated.</li></ul><h3><strong>4. Waters Corporation: Waters Aura Systems</strong></h3><ul><li>Brochure</li><li><a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/pdf/720009268_7b9ad02cb4.pdf"><strong>Full PDF for download</strong></a></li></ul><p>The presentation introduces the <strong>Waters Aura Systems</strong>, a family of high-throughput, fluidics-free instruments for the characterization and identification of visible and subvisible particles. All Aura platforms provide particle counting, identification, morphology assessment, and flexible sample volumes ranging from microliters to milliliters. The portfolio includes configurations tailored to different applications: <strong>AuraBMI</strong> for biologics particle analysis, <strong>Aura</strong> for particle analysis with identification, <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/2437"><strong>AuraPTx</strong></a> for protein formulation development, <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/2438"><strong>AuraGT</strong></a> for gene therapy, <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/2439"><strong>AuraCL</strong></a> for cell therapy, and <a target="_blank" rel="noopener noreferrer" href="https://labrulez.com/en-us/all/products/2190"><strong>Aura+</strong></a> as the most comprehensive platform. The systems are designed for automation-ready operation, straightforward method transfer, and continuity from research through QC.</p><p>A key feature of the Aura platform is the combination of <strong>Backgrounded Membrane Imaging (BMI), Fluorescence Membrane Microscopy (FMM), and Side Illumination Membrane Imaging (SIMI)</strong>. BMI captures particles on a membrane and subtracts the membrane background to improve particle contrast, while FMM uses fluorescent dyes or conjugated antibodies to distinguish specific particle types. This enables differentiation of protein aggregates, cells, viral capsids, degraded excipients, plastics, fibers, and other contaminants that may look similar based on morphology alone. SIMI adds further information for identifying unlabeled inorganic particles such as glass, fibers, and Dynabeads. Together, these techniques provide more specific particle identification than morphology-based classification alone.</p><p>The systems are particularly suited to <strong>biologics, gene therapy, and cell therapy development</strong>. For gene therapy, Aura can evaluate AAV stability, distinguish capsid-related particles, and monitor DNA leakage using SYBR Gold fluorescence, with measurements possible from as little as <strong>5 µL of sample</strong>. For cell therapy, the system can differentiate single cells, cell aggregates, protein aggregates, and extrinsic particles. The platform also supports flexible sample volumes and 24- or 96-well membrane formats, allowing the same general approach to be used from sample-limited early development through larger-volume and QC workflows. The brochure reports excellent quantitative linearity across serial dilutions and emphasizes the ability to preserve sample for additional orthogonal analyses.</p><p>From a technical perspective, Aura Systems provide <strong>100% sampling efficiency</strong>, a particle detection and quantitation range above <strong>1 µm</strong>, and can handle concentrations above <strong>3,000,000 particles/mL</strong> for 1.6 µm particles. Brightfield membrane imaging takes approximately <strong>one minute per sample</strong>, while fluorescence measurements require about <strong>15–30 seconds per sample</strong>. The instruments are compatible with robotic automation and offer different fluorescence-channel configurations depending on the selected Aura model. Overall, the platform is positioned as a comprehensive solution for obtaining quantitative particle counts together with information on particle identity and composition across the development and quality-control lifecycle.</p>

News from LabRulezICPMS Library - Week 36, 2026

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Thermo Scientific ITEX Dynamic Headspace Tool 

Thermo Scientific ITEX Dynamic Headspace Tool enables automated VOC enrichment with ppt sensitivity using dynamic headspace for GC workflows.

<p><strong>The Thermo Scientific™ ITEX Dynamic Headspace Tool is an autosampler accessory for the</strong><a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/63"><strong> TriPlus™ RSH </strong></a><strong>and </strong><a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/422"><strong>TriPlus RSH SMART</strong></a><strong> Autosamplers designed for the enrichment of volatile organic compounds (VOCs) using dynamic headspace technology. It enables ppt-level sensitivity and allows sample enrichment to be easily integrated into an automated gas chromatography (GC) workflow.</strong></p><ul><li>The ITEX-DHS technique uses a gas-tight syringe to collect the headspace and a microtrap inside the syringe needle to efficiently trap and concentrate VOCs through repeated syringe strokes.&nbsp;</li><li>Sensitivity can be scaled according to the number of strokes, making the method suitable for both low- and high-concentration samples.&nbsp;</li><li>The system is designed for easy method set-up with only a few parameters, simple access to the trap, and excellent robustness for long-term operation.&nbsp;</li><li>A closed system removes any risk of breakthrough.&nbsp;</li><li>Independent trap desorption temperature and flow control maximize desorption efficiency without affecting GC inlet settings.&nbsp;</li><li>When used with the TriPlus RSH SMART autosampler, the SMART gas-tight syringe enables automatic usage traceability.&nbsp;</li><li>The entire automated workflow can be fully controlled through <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/76"><strong>Thermo Scientific™ Chromeleon™ CDS</strong></a>.</li></ul><p>For VOC analysis in many liquid and solid samples, ITEX offers a valuable alternative to classical enrichment techniques by combining ease of use with robust performance.</p><h3><strong>Key features</strong></h3><ul><li>Dynamic headspace VOC enrichment with<strong> ppt-level sensitivity</strong></li><li><strong>Easy integration</strong> into automated GC workflows</li><li><strong>Gas-tight syringe and microtrap</strong> in the needle for efficient analyte concentration</li><li><strong>Scalable sensitivity</strong> based on the number of syringe strokes</li><li><strong>Easy method set-up</strong> with few parameters</li><li><strong>Robust design </strong>for long-term operation</li><li><strong>Closed system</strong> minimizing the risk of breakthrough</li><li><strong>Independent desorption</strong> temperature and flow control</li><li><strong>Automatic usage</strong> traceability with SMART gas-tight syringe</li><li>Full control through <strong>Chromeleon CDS</strong></li></ul><h3><strong>Technical specifications</strong></h3><ul><li><strong>Description: </strong>includes SMART gas-tight syringe, focusing trap, built-in trap heating, cooling fan, and trap cleaning capability</li><li><strong>Application: </strong>enrichment of volatile organic compounds (VOCs)</li><li><strong>Compatible equipment: </strong><a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/63"><strong>TriPlus RSH</strong></a> and <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/422"><strong>TriPlus RSH SMART </strong></a>Autosamplers</li><li><strong>Type:</strong> autosampler accessory</li><li><strong>Unit size: </strong>each</li></ul>

Thermo Scientific Vanquish Sample Hub

Increase sample capacity for extra-long unattended operation with an intelligent robotic that automates sample loading in the Thermo Scientific™ Vanquish™ UHPLC system.

<p><strong>The Thermo Scientific™ Vanquish™ Sample Hub integrates seamlessly with the </strong><a target="_blank" rel="noopener noreferrer" href="https://lcms.labrulez.com/products?category=40&amp;manufacturerItems=3&amp;search=Vanquish"><strong>Vanquish™ UHPLC platform</strong></a><strong>, providing fully automated robotic sample handling for high-throughput laboratories. Supporting up to 8,832 samples (23 well plates), it enables extended unattended operation by automatically transferring samples to the UHPLC system.&nbsp;</strong></p><p>Controlled environmental conditions help preserve sample integrity, while the integrated barcode reader continuously tracks racks and well plates whenever the door is closed, allowing new samples to be added without interrupting ongoing analyses.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_Vanquish_Sample_Hub_4_4458a169d1.jpg" alt="Thermo Scientific Vanquish Sample Hub" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_Vanquish_Sample_Hub_4_4458a169d1.jpg 211w," sizes="100vw" width="650" height="481"></p><h4><strong>Key Features</strong></h4><ul><li>Supports up to <strong>8,832 samples</strong> for long-term unattended operation</li><li>Monitor and manage an inventory of up to <strong>9 sample racks, deep well plates, or 20 shallow well plates (15mm height) in SBS format</strong></li><li>Protects sample quality through controlled environmental conditions and innovative air-stream cooling</li><li>Integrated barcode reader enables automated inventory management, rack and plate verification, and empty shelf detection</li><li>Allows samples to be added while analyses are running without stopping the UHPLC system</li><li>Fully integrated with <a target="_blank" rel="noopener noreferrer" href="https://lcms.labrulez.com/products/76"><strong>Thermo Scientific™ Dionex™ Chromeleon™ Chromatography Data System (CDS)</strong></a> for familiar instrument control</li></ul><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_Vanquish_Sample_Hub_3_5a881d0af1.jpg" alt="Thermo Scientific Vanquish Sample Hub " srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_Vanquish_Sample_Hub_3_5a881d0af1.jpg 236w," sizes="100vw" width="650" height="430"></p><h4><strong>Specifications</strong></h4><ul><li><strong>GLP Features:</strong> All System Parameters Logged in The <a target="_blank" rel="noopener noreferrer" href="https://lcms.labrulez.com/products/76"><strong>Chromeleon Chromatography Data System Audit Trail</strong></a></li><li><strong>Includes:</strong> Barcode reading: Empty shelf level detection, Rack/well plate verification, Inventory management</li><li><strong>Overall Depth (English):</strong> 24.4 in.</li><li><strong>Overall Depth (Metric):</strong> 620 mm</li><li><strong>Overall Height (English):</strong> 31.7 in.</li><li><strong>Overall Height (Metric):</strong> 804 mm</li><li><strong>Overall Width (English):</strong> 13.3 in.</li><li><strong>Overall Width (Metric):</strong> 339 mm</li><li><strong>PC Connection:</strong> USB 2.0</li><li><strong>Safety Features:</strong>&nbsp;<ul><li>Sample rack/well plate detection sensor on shovel</li><li>Barcode reader to detect sample rack/well plate type and shelf ID</li><li>Automatic stop when door is opened (interlock door switch)</li><li>Automatic opening of door after power failure&nbsp;</li><li>3 LEDs for status monitoring</li><li>Active evaporation system for condensation</li></ul></li><li><strong>Temperature Range:</strong>&nbsp;<ul><li>4°C to 40°C (≥22 K Below Ambient (at &lt;80% RH)</li><li>Accuracy -2°C to +2°C (at 25°C, 50% RH)</li><li>Stability ±0.5°C (at 25°C, 50% RH))</li></ul></li><li><strong>Voltage:</strong> 100/240 V</li><li><strong>Weight (Metric):</strong> &lt;38.5 kg</li><li><strong>Type:</strong> Vanquish Sample Hub Without Shelf and Racks</li></ul><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_Vanquish_Sample_Hub_2_e65f12f12e.jpg" alt="Thermo Scientific Vanquish Sample Hub " srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_Vanquish_Sample_Hub_2_e65f12f12e.jpg 224w," sizes="100vw" width="650" height="452"></p>

Thermo Scientific TriPlus™ RSH SMART Autosampler

Extend automation, performance, and versatility for GC and GC/MS applications, while ensuring easier and safer operations through SMART consumables ID recognition and usage tracking.

<div><div id="product-description"><p><strong>Expand automated sampling capabilities beyond liquid, headspace, and solid phase microextraction (SPME) injections. The advanced, built-in robotics of the Thermo Scientific™ TriPlus™ RSH SMART Autosampler deliver exceptional precision, sample handling flexibility, and reliable unattended operation. Enabling SMART consumables tracking, it offers easier, safer and traceable operations. Accurate and repeatable sample preparation and injection are essential to achieving the highest quality GC/GC-MS results. Enhance data quality and laboratory efficiency by automating your entire sample handling workflow.</strong></p></div><div><p>The TriPlus RSH SMART Autosampler brings together technological innovations that further expand automation, performance and versatility for GC and GC-MS applications, while ensuring easier and safer operations through SMART consumables ID recognition and usage tracking. Automated high-precision sample handling eliminates the manual labor and downtime typically required for tasks as standard/sample dilutions, internal standard addition and derivatization.</p><h3><strong>SMART Consumables</strong></h3><p>Validated SMART consumables are equipped with unique SMART chip storing parameters, ranges and usage history; enabling full traceability of sample preparation down to the syringe.</p><h3><strong>Automatic Syringe Changeout</strong></h3><p>Automatic Tool Change (ATC) capability automates the use of different syringes for sample preparation steps or different injection techniques within the sequence.</p><h3><strong>Vial Bottom Sensing Expands Application Range</strong></h3><p>Precise detection of vial bottoms enables the autosampler to accurately withdraw from sample amounts as little as 5 μL, enhancing data quality of sample-limited applications.</p><h3><strong>Flexible liquid sample handling</strong></h3><p>Optimized liquid injection modes and customizable syringe filling techniques, support a wide range of sample types and full GC inlet compatibility.</p><h3><strong>Automated headspace injection for volatile analysis</strong></h3><p>High temperature gas-tight syringe allows direct headspace injection into the GC inlet for increased injection volume flexibility. Sample vial capacity of up to 300x 10 mL/20 mL vials and sample incubation overlapping, facilitate long unattended operation.</p><h3><strong>Automated, solvent-free SPME</strong></h3><p>Precise control of all steps—fiber preconditioning, adsorption and desorption, as well as fiber washes—delivers maximum performance for SPME applications. Boost productivity with the optimized SPME Arrow design. It offers optimized fiber geometry to achieve 10x superior sensitivity compared to classical SPME, 2x faster extraction time and superior robustness.</p><h3><strong>Automated Sample Preparation</strong></h3><p>The Triplus RSH SMART Autosampler combines highly versatile sample injection capability with automated sample preparation procedures, eliminating typical GC-MS workflow bottlenecks. Daily operations ranging from sample/standard dilution to more complex derivatization protocols, can be fully automated and easily programmed with the Sampling Workflow Editor Software.</p><h3><strong>Extend productivity with the optional 1D barcode reader</strong></h3><p>The optional 1D barcode reader eliminates the need to log and track sample information manually; enabling you to streamline internal operations, save time, increase efficiency, and reduce errors.</p><h3><strong>Specifications</strong></h3><ul><li><strong>Type: </strong>TriPlus RSH SMART Standard Liquid, Regular Rail</li><li><strong>Sample Capacity:</strong> 4608 Well Plates, 840 x 0.5 mL or 0.7 mL Vials, 648 x 2 mL Sample Vials, 240 x 10 mL or 20 mL Vials</li><li><strong>Injection Mode: </strong>8 Fully Customizable Method-Specific Injection Mode Presets</li><li><strong>Injection Speed:</strong> Selectable from 0.1 μL/s to 2000 μL/s</li><li><strong>Injection Volume: </strong>0.1 to 10,000 μL</li><li><strong>Description: </strong>TriPlus RSH SMART configured for liquid injection on regular X-axis length. Only for manual tool change. Complete with liquid syringe tool, 2 x 10 μL SMART syringes, standard washing station and a single tray holder with 3 trays for 2 mL vials. Expandible to other sampling techniques (Headspace, SPME, SPME Arrow, ITEX-DHS) and with sample preparation tools.</li><li><strong>Tool Exchange:</strong> Only for manual tool exchange. No tool park station.</li><li><strong>For Use With (Equipment):</strong> Compatible with Smart syringes/fibers only.</li></ul></div></div>

Thermo Scientific™ AI/AS 1610 Liquid Autosampler

 The Thermo Scientific AI/AS 1610 Liquid Autosampler boosts throughput with efficient, safe sample processing and a user-friendly design ideal for busy labs.

<div><div id="product-description"><p><strong>Enhance liquid sampling automation for your gas chromatography (GC) applications with simplicity and robustness. Designed to meet the demands of any busy high-throughput lab, the Thermo Scientific™ AI/AS 1610 Liquid Autosampler will help to process more samples efficiently and safely with its advanced design and usability features, greatly enhanced for easy adoption for both beginners and experienced users.&nbsp;</strong></p><p>With the possibility to expand to <strong>up to a 310-sample capacity </strong>with <strong>simultaneous dual-tower operations</strong>, the AI/AS 1610 offers the fit-for-purpose solution to budget-conscious laboratories looking for reliable automation of liquid samples injection into a<strong> GC or GC-MS system. </strong>The Thermo Scientific™ AI/AS 1610 Liquid Autosampler combine <strong>performance, simplicity, and robustness for your everyday workflow.</strong></p><h5><strong>The AI/AS 1610 Liquid Autosampler</strong> is available in <strong>two models:&nbsp;</strong></h5><ul><li>the upgradable<strong> 8-vial capacity AI 1610</strong>&nbsp;</li><li>the<strong> 155-vial capacity AS 1610&nbsp;</strong></li></ul><p>Both offer the<strong> dual-tower Gemini configuration for simultaneous injection in two channels.</strong></p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Pragolab_Autosampler_AI_1610_s_kapacitou_8_nebo_155_vzorku_9d37f0ea9a/Pragolab-Autosampler-AI-1610-s-kapacitou-8-nebo-155-vzorku.jpg" alt="Thermo Scientific™ AI/AS 1610 Liquid Autosampler:  8-vial capacity and 155-vial capacity AI 1610 " srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Pragolab_Autosampler_AI_1610_s_kapacitou_8_nebo_155_vzorku_9d37f0ea9a/thumbnail_Pragolab-Autosampler-AI-1610-s-kapacitou-8-nebo-155-vzorku.jpg 245w," sizes="100vw" width="1097" height="666"></p><h3><strong>Enhanced Usability</strong></h3><ul><li><strong>Easy set up</strong> through self-aligning, not requiring any position adjustment</li><li><strong>Easy slide-in installation and free access to the injector </strong>for maintenance</li><li><strong>Easy syringe viewing and replacement</strong> with illuminated compartment and magnifier lens</li><li>Enhanced <strong>color-coded instrument status indication</strong></li><li><strong>Safe operation</strong> with automatic selection of the best injection settings through recognition of the injector type and injection mode</li><li><strong>Simplified connectivity </strong>with a single cable including communication, synchronization and power supply</li></ul><h3><strong>Enhanced Sample Throughput</strong></h3><ul><li><strong>Wide sample capacity scalability</strong> to fit any workload demand</li><li><strong>Dual Tower Gemini</strong> for upmost productivity with simplified configuration and connectivity</li></ul><h3><strong>Enhanced Performance</strong></h3><ul><li>Expanded applicability with liquid sample volume <strong>injections up to 80 μL</strong></li><li>Free pre- and post injection syringe rinsing with single or combined solvents (up to four) virtually <strong>eliminates sample carry-over</strong></li><li><strong>Efficient, accurate sampling</strong> <strong>of low boiling compounds</strong> with the syringe kept away from the inlet’s temperature influence</li><li><strong>Seamless integration into Thermo Scientific™ chromatography software</strong></li></ul><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Pragolab_Dizajn_autosampleru_Thermo_AI_AS_1610_pro_snadny_pristup_k_injektoru_GC_0b1d294ab5/Pragolab-Dizajn-autosampleru-Thermo-AI-AS-1610-pro-snadny-pristup-k-injektoru-GC..jpg" alt="Thermo Scientific™ AI/AS 1610 Liquid Autosampler" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Pragolab_Dizajn_autosampleru_Thermo_AI_AS_1610_pro_snadny_pristup_k_injektoru_GC_0b1d294ab5/thumbnail_Pragolab-Dizajn-autosampleru-Thermo-AI-AS-1610-pro-snadny-pristup-k-injektoru-GC..jpg 245w," sizes="100vw" width="1090" height="520"></p><h3><strong data-start="105" data-end="123">Specifications</strong></h3><ul><li><strong data-start="126" data-end="146">Sample Capacity:</strong> 8 x 2 mL Vials</li><li><strong data-start="164" data-end="183">Injection Mode:</strong> Automatically selected and optimized according to injector type</li><li><strong data-start="250" data-end="270">Injection Speed:</strong> Fast/Slow/Variable (1 to 60,000.00 μL/min)</li><li><strong data-start="317" data-end="338">Injection Volume:</strong> 0.01 to 80 μL</li><li><strong data-start="355" data-end="371">Description:</strong> AI 1610 Liquid Autosampler for TRACE 1600 Series GC</li><li><strong data-start="426" data-end="447">Washing Solvents:</strong> Up to 4</li><li><strong data-start="458" data-end="471">Quantity:</strong> Each</li><li><strong data-start="479" data-end="493">Unit Size:</strong> Each</li></ul><figure class="image"><img style="aspect-ratio:650/434;" src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_AI_AS_1610_Liquid_Autosampler_37e5c32f69.jpg" alt="Thermo Scientific™ AI/AS 1610 Liquid Autosampler" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_AI_AS_1610_Liquid_Autosampler_37e5c32f69.jpg 234w," sizes="100vw" width="650" height="434"></figure></div></div>

Thermo Scientific™ TriPlus™ RSH Autosampler

Robotic GC autosampler with multimode injection, tool exchange, and full sample prep automation. Enables 24/7 workflows for food, environmental, and forensic labs.

<h4><strong>Flexible, high-capacity autosampler for GC and GC-MS with advanced sample prep automation</strong></h4><p><strong>The TriPlus RSH Autosampler is a versatile robotic sampling platform designed to maximize automation, precision, and productivity in gas chromatography workflows. Fully compatible with Thermo Scientific™ GC and GC-MS systems, it supports liquid, headspace (HS), and SPME/SPME Arrow injections, with optional modules for µSPE, ITEX-DHS, and automated sample preparation. The unique Automatic Tool Change (ATC) system allows the autosampler to switch between up to six syringes in a single sequence, enabling unattended workflows for complex multistep protocols.</strong></p><h3><strong>Key Features and Benefits</strong></h3><h4>🧪 <strong>Multimode Injection and Sample Handling</strong></h4><ul><li>Supports liquid, headspace, SPME, SPME Arrow, and ITEX-DHS techniques</li><li>Switch between injection modes in a single sequence using ATC</li><li>Bottom vial sensing enables precise injections from as little as <strong>5 μL</strong> of sample</li></ul><h4>🔁 <strong>Automated Sample Preparation</strong></h4><ul><li>Perform dilution, standard addition, derivatization, and internal standard workflows</li><li>Tools: Vortexer, Incubator, Heatex-Stirrer, Dilutor, µSPE module</li><li>Visual drag-and-drop <strong>Sampling Workflow Editor</strong> for custom prep protocols</li></ul><h4>📦 <strong>High Throughput and Capacity</strong></h4><ul><li>Unattended operation with up to <strong>972 × 2 mL vials</strong> or <strong>840 × 0.7 mL vials</strong></li><li>Extended X-arm option for larger trays and accessory support</li><li>Dual-GC configurations with Clone Mode or DoublePro setups</li></ul><h4>⚙️ <strong>Precision and Flexibility</strong></h4><ul><li>Automated Tool Change (ATC): Up to <strong>6 tools</strong> in one sequence</li><li>Injection volume range: <strong>0.1 μL to 10 mL</strong></li><li>Compatible with all major GC injector types (SSL, PTV, OC, PKD, PPKD)</li></ul><h4>🧠 <strong>Smart Software and Control</strong></h4><ul><li>Fully integrated with <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/76"><strong>Chromeleon™</strong></a>,<a target="_blank" rel="noopener noreferrer" href="https://lcms.labrulez.com/products/1758"><strong> Xcalibur™</strong></a>, and <strong>Chrom-Card™ CDS</strong></li><li>Local controller or virtual terminal control interface</li><li>Barcode readers for full sample tracking</li></ul><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/application::product.product/Thermo-TriPlus-RSH-Autosampler-1.jpg" alt="Thermo Scientific™ TriPlus™ RSH Autosampler" width="null" height="null"></p><h3><strong>Applications</strong></h3><ul><li><strong>Food safety</strong>: Trace analytes, contaminants, derivatization (e.g. FAMEs, dioxins)</li><li><strong>Environmental</strong>: VOCs, SVOCs, POPs, air toxics</li><li><strong>Forensics &amp; clinical</strong>: Biological matrices, explosive residues, drugs</li><li><strong>Chemical industry</strong>: Routine QC, trace impurities, residual solvents</li><li><strong>High-throughput labs</strong>: 24/7 unattended workflows with complex prep steps</li></ul><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/application::product.product/QExactive-GCMSMS-Orbitrap-with-Autosampler-sideangle-1856x1391.jpg-650.jpg" alt="Thermo Scientific™ TriPlus™ RSH Autosampler" width="null" height="null"></p>

Thermo Scientific™ TriPlus™ 500 GC Headspace Autosampler

Powered by a completely new design, the Thermo Scientific™ TriPlus™ 500 Headspace Autosampler delivers reliability and robustness for testing laboratories performing volatiles analysis.

<p><strong>Powered by a completely new design, the Thermo Scientific™ TriPlus™ 500 Headspace Autosampler delivers reliability and robustness for testing laboratories performing volatiles analysis.</strong></p><p>Valve-and-loop technology and <strong>other innovative features</strong> ensure that this autosampler streamlines daily workflows, saving time with reliable unattended operation, optimizing sample throughput with expanded vial capability, and facilitating method portability with powerful software. Smartly integrated with the <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/483"><strong>Thermo Scientific™ TRACE™ 1600 Series GC</strong></a><strong>,</strong> this modular platform provides today's analytical testing and services laboratories with the productivity needed to succeed.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Pragolab_Schematicke_znazorneni_nastriku_pomoci_Head_Space_autosampleru_Thermo_Tri_Plus_500_fd64009b8a/Pragolab-Schematicke-znazorneni-nastriku-pomoci-HeadSpace-autosampleru-Thermo-TriPlus-500.jpg" alt="Thermo Scientific™ TriPlus™ 500 GC Headspace Autosampler: Valve-and-loop headspace injection principle" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Pragolab_Schematicke_znazorneni_nastriku_pomoci_Head_Space_autosampleru_Thermo_Tri_Plus_500_fd64009b8a/thumbnail_Pragolab-Schematicke-znazorneni-nastriku-pomoci-HeadSpace-autosampleru-Thermo-TriPlus-500.jpg 245w," sizes="100vw" width="1812" height="560"></p><h4><strong>Reliability for analytical testing and services laboratories and versatility for research and method development.</strong></h4><p>The new design of the TriPlus 500 Headspace Autosampler incorporates innovative features for highly accurate analytical results, including:</p><h5><strong>New pneumatic controls for high precision and robustness</strong></h5><ul><li><strong>Best injection repeatability</strong> for consistent results at every run.</li><li><strong>No carryover </strong>due to effective sample path purging.</li><li><strong>Automatic leak check </strong>during injection to ensure safe runs.</li></ul><figure class="image"><img style="aspect-ratio:681/480;" src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_Tri_Plus_500_GC_Headspace_Autosampler_2_62a58c525f.jpg" alt="Thermo Scientific™ TriPlus™ 500 GC Headspace Autosampler: Long Sequence Area Counts Repeatability. 120 consecutive headspace injections of a 50 ppm ethanol solution in water (5 ml in 10 ml crimp top vial). Overall RSD%=0.7" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_Tri_Plus_500_GC_Headspace_Autosampler_2_62a58c525f.jpg 221w," sizes="100vw" width="681" height="480"></figure><h5><strong>Best sample integrity and ease-of-use via direct column connection</strong></h5><ul><li><strong>A shorter sample path</strong> for high inertness towards polar compounds.</li><li><strong>Expanded high temperature</strong> <strong>applicability</strong> <strong>with higher recovery </strong>of high boiling point compounds.</li><li><strong>Simplified method set up </strong>with no transfer line and injector temperature settings required.</li></ul><figure class="image"><img style="aspect-ratio:720/484;" src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_Tri_Plus_500_GC_Headspace_Autosampler_3_a7e8932898.jpg" alt="Thermo Scientific™ TriPlus™ 500 GC Headspace Autosampler: Recovery of a standard hydrocarbon mixture C10-C40 at high temperature operation, showing >60% recovery at 300°C" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_Tri_Plus_500_GC_Headspace_Autosampler_3_a7e8932898.jpg 232w," sizes="100vw" width="720" height="484"></figure><h5><strong>Compact yet scalable design for better laboratory efficiency and productivity</strong></h5><ul><li>Compact HS-GC design saves<strong> 30%</strong> of valuable bench space.</li><li>Tailored throughput requirements with in-field scalability from<strong> 12 to 240 vials</strong>, requiring no additional space and no compromise on performance.</li><li>Faster sample equilibration with the new <strong>Quick Spin Shaking design</strong> for maximal sensitivity in a shorter cycle time.</li></ul><h5><strong>Comprehensive HS-GC configuration solution</strong></h5><ul><li>Available with<strong> direct column connection</strong> or transfer line for maximum configuration flexibility.</li><li>When a direct column connection is not possible, the autosampler configured with a transfer line maintains <strong>high precision, efficient sample transfer.</strong></li><li>When configured with a transfer line, the TriPlus 500 HS autosampler<strong> </strong>is ideal for connecting to the <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/483"><strong>Thermo Scientific™ TRACE™ 1600 Series GC</strong> </a>with auxiliary oven or for connection to third-party GC instruments</li><li>The TriPlus 500 HS with transfer line allows <strong>combined headspace and liquid injection</strong> in the same column, through operation with the <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/70"><strong>TriPlus 100 LS </strong></a><strong>or TriPlus RSH or</strong><a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/422"><strong> RSH SMART</strong></a><strong> autosampler on the same GC.</strong></li></ul><h5><strong>Software and system checks for compliance and data integrity</strong></h5><ul><li>Integrated with <strong>Thermo Scientific™ Chromeleon™ CDS software</strong>, Title 21 CFR Part 11-compliant.</li><li>Easy analytical system performance qualification with the IQ/OQ/PQ Qualification Wizard and daily sequence performance checks with the System Suitability Test Wizard.</li></ul><h4><strong data-start="0" data-end="18" data-is-only-node="">Specifications</strong></h4><ul><li><strong data-start="21" data-end="30">Type:</strong> TriPlus™ 500 GC Headspace Autosampler</li><li><strong data-start="71" data-end="91">Sample Capacity:</strong> 12 Vials, Upgradable to 120 and 240 Vials</li><li><strong data-start="136" data-end="155">Injection Mode:</strong>&nbsp;<ul><li>Standard</li><li>Multiple Headspace Extraction (MHE)</li><li>Multiple Headspace Injection (MHI)</li></ul></li><li><strong data-start="240" data-end="256">Description:</strong> TriPlus™ 500 Headspace Autosampler with Direct Column Connection</li><li><strong data-start="324" data-end="337">Software:</strong> Thermo Scientific™ Chromeleon CDS, Thermo Scientific™ TraceFinder, and Thermo Scientific™ XCalibur Software</li><li><strong data-start="448" data-end="477">For Use With (Equipment):</strong> <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/products/483">Trace 1600 Series</a></li><li><strong data-start="498" data-end="511">Quantity:</strong> Each</li><li><strong data-start="519" data-end="533">Unit Size:</strong> Each</li></ul>

Thermo Scientific AI/AS 1310 liquid sampling automation

The AI/AS 1310 autosampler series offers 8 to 155-position capacity for GC liquid injections, combining robustness and ease of use for both QA/QC and high-throughput labs.

<p><strong>As the next evolution in sampling automation, the Thermo Scientific™ AI/AS 1310 Series autosampler is the optimum choice for gas chromatography liquid injections. Ranging from an 8-position system (AI 1310 Autoinjector) to a 155 sample capacity autosampler (AS 1310), these systems are engineered to meet the highest requirements of ruggedness and ease of use and fulfill the needs of both QA/QC and high-throughput environments.</strong></p><h4><strong>Syringe thermal stability</strong></h4><p>The syringe is kept away from the inlet’s temperature influence so that efficient sampling of low boiling compounds is preserved.</p><h4><strong>Cross-contamination free</strong></h4><p>Pre- and Post-injection syringe rinsing with single or combined solvents (A, B, C, D, A+B, C+D) makes carry-over negligible.</p><h4><strong>System upgradability</strong></h4><p>An upgrade option is available for AI 1310 to extend its sample throughput to the 155 sample capacity of the AS 1310 autosampler.</p><h4><strong>System control</strong></h4><p>All necessary electronics are on board the sampling module. Both AI 1310 and AS 1310 can be controlled through the data system set-up menu.</p><h4><strong>System setup</strong></h4><p>Easy self-aligning, slide-in installation does not require any turret/syringe adjustment over the injector or the sample vial.</p><h4><strong>RoHS compliance</strong></h4><p>The AI/AS 1310 is compliant with the latest Restriction of Hazardous Substances (RoHS) requirements for hazardous substances in electrical and electronic equipment.</p><h4><strong>Removable trays</strong></h4><ul><li><strong>AI 1310 - The 8-position sample holder </strong>can easily be removed and replaced by another one. Each sample holder can be specifically labeled and used for sample preparation or storing.</li><li><strong>AS 1310 - The 155-position rotating carousel</strong> can be easily removed and replaced for sample preparation or storage if required.</li></ul><h4><strong>AS 1310 Gemini kit</strong></h4><p>Simply and easily automate simultaneous injections on two channels on the Thermo Scientific gas chromatographs, for double the productivity.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/application::product.product/Thermo-Trace-1310-GC-System-1.jpg" alt="Thermo Scientific AI/AS 1310 liquid sampling automation" width="null" height="null"></p><h3><strong>System specifications</strong></h3><h4><strong>Sample loading capacity</strong></h4><ul><li>8 (AI 1310)</li><li>155 (AS 1310)</li><li>310 (AS 1310 Gemini Configuration on Thermo Scientific TRACE™ 1300 GC, TRACE 1310 GC, and TRACE GC Ultra)</li><li><strong>Vial capacity: </strong>2 mL</li><li><strong>Optional micro-volume vials: </strong>300 µL</li><li><strong>Injections/vial:</strong> 0-99</li><li><strong>Viscosity delay: </strong>Yes/No</li></ul><h4><strong>Syringes</strong></h4><ul><li><strong>Standard</strong>: 10 µL</li><li><strong>Optional Micro-volume: </strong>5 µL</li><li><strong>Optional Nano-volume:</strong> 0.5 µL</li></ul><h4><strong>Injection parameters</strong></h4><ul><li><strong>Maximum volume: </strong>5 µL</li><li><strong>Minimum volume:</strong> 0.01 µL</li><li>Increments 0.01 µL steps</li></ul><h4><strong>Syringe rinsing</strong></h4><ul><li>Pre- and/or Post-injection</li><li><strong>Solvent selection:</strong> Single or combined mode</li><li>Sample pre-washes</li><li>Bubble elimination</li><li><strong>Solvent bottles</strong>: 4 x 4 mL</li><li><strong>Waste bottle capacity: </strong>40 mL</li></ul><h3><strong>Pre-set injection modes</strong></h3><h4><strong>“Minimum” needle depth</strong></h4><p>With this option, the syringe needle penetrates only partially in the inlet. Pre- and Post-injection dwell times are automatically set to zero. This selection enables “Cold Needle” type injections, preventing sample pre-volatilization from the needle. When operating in “Minimum” injection depth mode, all parameters are optimized and preset (Needle depth, pre- and post-dwell time, and Injection speed). Fast injection speed is optimized for this technique.</p><h4><strong>“Standard” needle depth</strong></h4><p>Using this option, the syringe needle penetrates entirely in the inlet. This selection offers the choice of pre- and post-injection injection dwell times, allowing to perform Hot Empty Needle type injections with the SSL inlet. This technique does not require any packing material in the liner. It should be preferred when analyzing thermally-labile compounds. Preset parameters are needle depth and injection speed. Manually set parameters are pre- and post-injection injection dwell times.</p><h4><strong>Reproducibility</strong></h4><p><strong>Chromatographic performance:</strong><br>&lt; 0.3 RSD % for C12, C16, C24 (C12-C24 alkane mix in hexane). Data obtained on 10 subsequent Splitless analyses, 1µL injected volume using “Standard” needle depth option.</p><h4><strong>Carryover</strong></h4><p>&lt; 0.001% measured by the residual area in a heptane blank following the injection of pure C14 and using 4 post-washes in combined solvents A+B.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/application::product.product/Thermo-TSQtm-9000-1300-as-1310.jpg" alt="Thermo Scientific AI/AS 1310 liquid sampling automation" width="null" height="null"></p>

Thermo Scientific™ TriPlus™ 100 LS Liquid Autosampler

Move to the simplicity of this X-Y-Z robotic autosampler. Able to accommodate most samples, the Thermo Scientific™ TriPlus™ 100 LS liquid autosampler completely and reliably automates liquid injections, from nanovolume to large sample volumes. 

<div><div id="product-description"><p>Move to the simplicity of this X-Y-Z robotic autosampler. Able to accommodate most samples, <strong>the Thermo Scientific™ TriPlus™ 100 LS liquid autosampler</strong> completely and reliably automates liquid injections, from <strong>nanovolume to large sample volumes.</strong> <strong>The precise movement control</strong> of the autosampler allows correct sampling and injection optimization even for <strong>highly viscous samples or very volatile solvents.</strong> <strong>Based on the robust and proven technology of the TriPlus RSH robotic autosampler, the TriPlus 100 LS increases liquid sample handling automation and throughput with ease.</strong></p></div><div><h3><strong>Labor saving</strong></h3><ul><li><strong>Extended unattended operations</strong> made possible by the wide sample storage and large solvent capacities</li><li><strong>High-Throughput Configuration</strong> is possible through a dual GC or GCMS set-up, with Double Pro or Confirmation injection mode</li><li>Rapid Mode for increased sample throughput starts <strong>the syringe washing cycle during the GC cooling phase</strong></li></ul><h3><strong>Versatilty</strong></h3><ul><li><strong>Select from different pre-optimized liquid injection modes </strong>for a wide range of applications</li><li><strong>Use with a full range of performance-enhancing accessories </strong>for liquid sample handling of the <strong>Thermo Scientific™ TriPlus™ RSH and RSH SMART platforms</strong> for additional simplicity and dependability</li><li><strong>Syringe Cleaning options</strong> allow to install multiple solvent stations and wxpand solvent and waste volumes</li><li><strong>Add module options </strong>including an agitator, vortexer, liquid-cooled tray holder, and Temperature-Controlled Drawer</li></ul><h3><strong>Easy operations</strong></h3><ul><li><strong>Eight fully customizable method-specific preset menus</strong> for different injection modes are available through the data systems to easily allow the highest flexibility in liquid samples injections</li><li><strong>Optional hand-held control device</strong> with 4 keys, round knob, and graphical LCD display for local control</li><li>Thermo Scientific chromatography data systems integrated with<strong> Virtual Terminal software </strong>to completely mimic the physical controller</li></ul><figure class="image"><img style="aspect-ratio:650/567;" src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Scientific_Tri_Plus_100_LS_Liquid_Autosampler_3_0238d1dc37.jpg" alt="Thermo Scientific™ TriPlus™ 100 LS Liquid Autosampler" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Scientific_Tri_Plus_100_LS_Liquid_Autosampler_3_0238d1dc37.jpg 179w," sizes="100vw" width="650" height="567"></figure><h3><strong>Specifications</strong></h3><ul><li><strong>Type:</strong> TriPlus 100 LS Liquid Autosampler</li><li><strong>Sample Capacity:</strong><ul><li>Up to 4608 well plates</li><li>Up to 840 0.5/0.7 mL vials</li><li>Up to 648 2 mL sample vials</li><li>Up to 180 10 mL or 20 mL vials</li></ul></li><li><strong>Injection Mode:</strong> 8 Fully Customizable Method-Specific Injection Mode Presets</li><li><strong>Injection Speed:</strong> Selectable from 0.1 µL/sec up to 900 µL/sec and fully programmable in three different steps, also dependent upon the volume of the installed syringe</li><li><strong>Injection Volume:</strong> 0.1 to 100.0 μL</li><li><strong>Description:</strong> Robotic XYZ Liquid Autosampler for GC and GCMS</li><li><strong>Tool Exchange:</strong> No tool exchange capability</li><li><strong>For Use With (Equipment):</strong> Compatible with standard and SMART syringes</li><li><strong>Quantity:</strong> Each</li><li><strong>Unit Size:</strong> Each</li></ul></div></div>

Products from category Sample injection from Thermo Fisher Scientific - page 1

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