Drug Screening in Non-Derivatized Urine by Automated Solid Phase Microextraction (SPME) and Comprehensive Multidimensional Gas Chromatography Time-of-Flight Mass Spectrometry (GCxGC-TOFMS)

® Forensic Toxicology Analysis of Non-derivatized Drugs in Urine by Automated Solid Phase Microextraction (SPME) GCxGC-TOFMS John Heim • LECO Corporation; Saint Joseph, Michigan USA Key Words: Non-Derivatized Drugs, Automated SPME, GCxGC-TOFMS This application presents experimental data from the forensics…

Life Science and Chemical Analysis Centre LECO Corporation, Saint Joseph, Michigan USA LSD 2ND DIMENSION RETENTION TIME (s) . Hydrocodone Application Snapshot Automated SPME-GCxGC-TOFMS Analysis of Non-Derivatized Drugs in Urine Oxycodone Diacetylmorphine Cocaine Ecstasy 6-Monoacetylmorphine Codeine Acetylcodeine Methamphetamine 1st DIMENSION…

Life Science and Chemical Analysis Centre LECO Corporation, Saint Joseph, Michigan USA Hydrocodone 7279 7279 7278 7277 1st Time (s) 2nd Time (s) 242 Peak # 7277 7278 7279 Name Cyclohexaneacetic acid, à-ethylUndeca-2,4,6,8,10-pentaenal, 11-(2-furyl)-, oxime Hydrocodone R.T. (s) 2500 ,…

® Delivering the Right Results Anti-Doping Control Using Comprehensive Multidimensional Gas Chromatography Time-of-Flight Mass Spectrometry (GCxGC-TOFMS) for Enhanced Detection of Anabolic Steroids in Urine John Heim, Doug Staples, and Joe Binkley • LECO Corporation, St. Joseph, MI Steroid Standards were…