Titration
IndustriesManufacturerMetrohm
Importance of the Topic
The accurate determination of acidity or basicity by titration remains a cornerstone of analytical chemistry. Modern potentiometric titrators like the 916 Ti-Touch improve reproducibility, user efficiency, and data integrity by integrating touchscreen operation, intelligent dosing units, and automated data management.
Objectives and Overview
This tutorial provides step-by-step guidance for setting up the 916 Ti-Touch, configuring titrants and sensors, creating titration methods, executing simple and advanced titrations, and managing multi-user access, using a dynamic pH titration as an example.
Used Instrumentation
- 916 Ti-Touch potentiometric titrator with touch-sensitive display
- 802 propeller stirrer or integrated magnetic stirring option
- 800 Dosino intelligent dosing unit or 805 Dosimat exchange unit
- pH electrodes (standard or intelligent iTrode via 854 iConnect)
- Buret tips, support rods, electrode holders
- USB or Ethernet printer interface
- Analytical balance via USB/RS-232 adapter
Methodology
- Mechanical installation: assembling stand, stirrer, electrode holder, dosing units, and tubing
- System configuration: registering titrants, sensors, printers, and balances
- Method creation: defining dosing devices, titrant properties, stop conditions, calculation templates, and report outputs
- Titration execution: cylinder conditioning (Prepare), live curve display, endpoint detection, and manual control options
- Data handling: sample entry via main dialog or sample table, automatic saving to USB/network, PC/LIMS report generation, and statistical evaluation
- User administration: single or multi-user login via password or ID profile, expert vs. routine dialog levels
Main Results and Discussion
The tutorial confirms that the 916 Ti-Touch offers intuitive touchscreen navigation, reliable hardware integration, and versatile software functionality. Automated endpoint recognition and live curve plotting ensure consistent titration performance, while built-in data export and reporting meet QA/QC demands.
Benefits and Practical Applications
- Efficient, reproducible acid–base analyses in research, quality control, and industrial laboratories
- Reduced training time and user errors through an intuitive graphical interface
- Comprehensive data management: on-device storage, USB export, network LIMS reporting, and PDF generation
- Customizable user access levels and audit trails for compliance in regulated environments
Future Trends and Potential Applications
Advances may include wireless IoT connectivity, deeper LIMS integration, AI-driven endpoint detection and method optimization, multi-parameter titrations (redox, complexometry), and cloud-based data analytics for remote monitoring and decision support.
Conclusion
The Metrohm 916 Ti-Touch combines modular hardware and flexible software to deliver a robust, user-friendly platform for both routine and advanced potentiometric titrations. Its comprehensive method configuration, automated data handling, and secure user management address the evolving needs of modern analytical laboratories.
Reference
- Metrohm AG. 916 Ti-Touch Tutorial, Article No. 8.916.8002EN, 03/2020.
Content was automatically generated from an orignal PDF document using AI and may contain inaccuracies.