Forensic Toxicology Analysis of Non-derivatized Drugs in Urine by Automated Solid Phase Microextraction (SPME) GCxGC-TOFMS

® Delivering the Right Results Drug Screening in Non-Derivatized Urine by Automated Solid Phase Microextraction (SPME) and Comprehensive Multidimensional Gas Chromatography Time-of-Flight Mass Spectrometry (GCxGC-TOFMS) Scott Pugh, John R. Heim, and Mark Libardoni • LECO Corporation, St. Joseph, Michigan Demonstrate…

Life Science and Chemical Analysis Centre LECO Corporation, Saint Joseph, Michigan USA LSD 2ND DIMENSION RETENTION TIME (s) . Hydrocodone Application Snapshot Automated SPME-GCxGC-TOFMS Analysis of Non-Derivatized Drugs in Urine Oxycodone Diacetylmorphine Cocaine Ecstasy 6-Monoacetylmorphine Codeine Acetylcodeine Methamphetamine 1st DIMENSION…

Life Science and Chemical Analysis Centre LECO Corporation, Saint Joseph, Michigan USA Hydrocodone 7279 7279 7278 7277 1st Time (s) 2nd Time (s) 242 Peak # 7277 7278 7279 Name Cyclohexaneacetic acid, à-ethylUndeca-2,4,6,8,10-pentaenal, 11-(2-furyl)-, oxime Hydrocodone R.T. (s) 2500 ,…

Life Science and Chemical Analysis Centre LECO Corporation, Saint Joseph, Michigan USA Xanax Application Snapshot SPME-GCxGC-TOFMS Non-Derivatized Sample Analysis for Drugs in Urine Oxycodone Methamphetamine Diacetylmorphine Codeine Cocaine SPME-GCxGC-TOFMS non-derivatized sample analysis of urine with positive identification of methamphetamine, cocaine,…